R*,R*-[α-(Phenylphosphino)isovaleraldehyde]pentacarbonyltungsten

Base Information

• Chemical Name: R*,R*-[α-(Phenylphosphino)isovaleraldehyde]pentacarbonyltungsten
• CAS No.: 91083-10-2
• Molecular Formula: C₁₆H₁₅O₆PW
• Molecular Weight: 518.115
• Mol file: 91083-10-2.mol

Synonyms:

Chemical Property of R*,R*-[α-(Phenylphosphino)isovaleraldehyde]pentacarbonyltungsten

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of R*,R*-[α-(Phenylphosphino)isovaleraldehyde]pentacarbonyltungsten

There total 1 articles about R*,R*-[α-(Phenylphosphino)isovaleraldehyde]pentacarbonyltungsten which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten (82265-64-3) + 1-morpholino-3-methyl-1-butene (53828-74-3) → R*,R*-[α-(Phenylphosphino)isovaleraldehyde]pentacarbonyltungsten (91083-10-2)

Guidance literature:

With water; In xylene; The mixt. of reagents in xylene was heated at 115°C for 5 h, hydrolized with H2O at 80°C, (Ar atm.);; chromy. on silica gel column with hexane-toluene; isomers were sepd. byrecrystn. from CH2Cl2-pentane;;

upstream raw materials:

syn-[5,6-dimethyl-2,3-bis(methoxycarbonyl)-7-phenyl-7-phosphanorbornadiene]pentacarbonyltungsten

1-morpholino-3-methyl-1-butene

Refernces