trimethyltin(IV)di(4-chlorobenzenesulfonyl)amide

Base Information

• Chemical Name: trimethyltin(IV)di(4-chlorobenzenesulfonyl)amide
• CAS No.: 155532-92-6
• Molecular Formula: C₁₅H₁₇Cl₂NO₄S₂Sn
• Molecular Weight: 529.052
• Mol file: 155532-92-6.mol

Synonyms:

Chemical Property of trimethyltin(IV)di(4-chlorobenzenesulfonyl)amide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of trimethyltin(IV)di(4-chlorobenzenesulfonyl)amide

There total 2 articles about trimethyltin(IV)di(4-chlorobenzenesulfonyl)amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

di(4-chlorobenzenesulfonyl)amine (2725-55-5) + trimethyltin(IV) hydroxide (56-24-6) → trimethyltin(IV)di(4-chlorobenzenesulfonyl)amide (155532-92-6)

Guidance literature:

In acetonitrile; byproducts: H2O; addn. of a soln. of Sn-compound to a suspn. of organic compound at 45°C with stirring; removing solvent, drying ( 1 hPa over P4O10), recrystn. (toluene/MeCN);

DOI:10.1016/0022-328X(94)80003-0

Reference yield: 44.0%

trimethyltin(IV)chloride (1066-45-1) + silver(I) di(4-chlorobenzenesulfonyl)amide (114206-08-5) → trimethyltin(IV)di(4-chlorobenzenesulfonyl)amide (155532-92-6)

Guidance literature:

In acetonitrile; byproducts: AgCl; addn. of a soln. of Sn-compound to a soln. of Ag-compound, 3 h at 50°C or 3 days at room temperature; filtn., removing solvent, recrystn. of residue (MeCN) at temperatures below 50°C, elem. anal.;

DOI:10.1016/0022-328X(94)80003-0

upstream raw materials:

trimethyltin(IV)chloride

silver(I) di(4-chlorobenzenesulfonyl)amide

di(4-chlorobenzenesulfonyl)amine

trimethyltin(IV) hydroxide

Refernces