1-Phenanthrol-d9

Base Information

• Chemical Name: 1-Phenanthrol-d9
• CAS No.: 922510-23-4
• Molecular Formula: C₁₄H₁₀O
• Molecular Weight: 203.161
• Mol file: 922510-23-4.mol

Synonyms:

Chemical Property of 1-Phenanthrol-d9

Chemical Property:

• Melting Point: 152-154°C (dec.)
• Storage Temp.: Refrigerator
• Solubility.: Chloroform (Slightly), Ethyl Acetate (Slightly)

Purity/Quality:

99% ^*data from raw suppliers

1-Phenanthrol-d9 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

• Uses: 1-Phenanthrol-d9 has been used as a reactant for the preparation of stable isotope-labeled internal standards of PAH metabolites from urine of smokers and nonsmokers.

Technology Process of 1-Phenanthrol-d9

There total 1 articles about 1-Phenanthrol-d9 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

decadeuterio-phenanthrene (1517-22-2) → 9-hydroxyphenanthrene-d9 + 2-hydroxyphenanthrene-d9 + 1-hydroxyphenanthrene-d9 (922510-23-4) + 3-hydroxyphenanthrene-d9

Guidance literature:

decadeuterio-phenanthrene; With Dichloromethyl methyl ether; tin(IV) chloride; In dichloromethane; at 20 ℃;

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 1h; Heating;

With potassium hydroxide; at 20 ℃; for 1h; Further byproducts given;

DOI:10.1021/ac060920l

upstream raw materials:

decadeuterio-phenanthrene

Refernces