7H-imidazo[4,5-c]tetrazo[1,5-a]pyridine

Base Information

• Chemical Name: 7H-imidazo[4,5-c]tetrazo[1,5-a]pyridine
• CAS No.: 1207615-07-3
• Molecular Formula: C₆H₄N₆
• Molecular Weight: 160.138
• Mol file: 1207615-07-3.mol

Synonyms:

Chemical Property of 7H-imidazo[4,5-c]tetrazo[1,5-a]pyridine

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 7H-imidazo[4,5-c]tetrazo[1,5-a]pyridine

There total 2 articles about 7H-imidazo[4,5-c]tetrazo[1,5-a]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

(2-chloro-pyridin-4-yl)-nitro-amine (14432-13-4) + 1-ethyl-3-methylimidazolium tetrafluoroborate (143314-16-3) → 7H-imidazo[4,5-c]tetrazo[1,5-a]pyridine (1207615-07-3)

Guidance literature:

With lithium azide; In water; N,N-dimethyl-formamide; at 20 - 80 ℃; for 6h; Product distribution / selectivity;

Reference yield: 95.0%

4-chloro-1H-imidazo[4,5-c]pyridine (2770-01-6) → 7H-imidazo[4,5-c]tetrazo[1,5-a]pyridine (1207615-07-3)

Guidance literature:

4-chloro-1H-imidazo[4,5-c]pyridine; With lithium azide; 1-ethyl-3-methylimidazolium tetrafluoroborate; In water; N,N-dimethyl-formamide; at 80 ℃; for 6h;

With hydrogen; palladium on activated charcoal; In water; N,N-dimethyl-formamide; Product distribution / selectivity;

Reference yield: 99.0%

7H-imidazo[4,5-c]tetrazo[1,5-a]pyridine (1207615-07-3) → 3-deazaadenine (6811-77-4)

Guidance literature:

7H-imidazo[4,5-c]tetrazo[1,5-a]pyridine; With hydrogenchloride; palladium 10% on activated carbon; In water; for 0.166667h;

With hydrogen; In water; for 36h; under 2280.15 Torr; Product distribution / selectivity;

upstream raw materials:

(2-chloro-pyridin-4-yl)-nitro-amine

1-ethyl-3-methylimidazolium tetrafluoroborate

4-chloro-1H-imidazo[4,5-c]pyridine

Downstream raw materials:

3-deazaadenine

Refernces