N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium bis(trifluoromethanesulfonyl)imide

Base Information

• Chemical Name: N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium bis(trifluoromethanesulfonyl)imide
• CAS No.: 1391034-56-2
• Molecular Formula: C₂F₆NO₄S₂*C₁₁H₂₄NO₂
• Molecular Weight: 482.466
• Mol file: 1391034-56-2.mol

Synonyms:

Chemical Property of N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium bis(trifluoromethanesulfonyl)imide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium bis(trifluoromethanesulfonyl)imide

There total 6 articles about N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium bis(trifluoromethanesulfonyl)imide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium iodide (1391034-52-8) + bis(trifluoromethane)sulfonimide lithium (90076-65-6) → N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium bis(trifluoromethanesulfonyl)imide (1391034-56-2)

Guidance literature:

In water; for 1h;

DOI:10.1002/jhet.876

Reference yield:

2-(2-methoxyethoxy)ethyl alcohol (111-77-3,95507-80-5) → N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium bis(trifluoromethanesulfonyl)imide (1391034-56-2)

Guidance literature:

Multi-step reaction with 4 steps

1: potassium hydroxide / diethyl ether / 10 h / 20 °C / Inert atmosphere

2: sodium iodide / acetone / 24 h / Inert atmosphere; Darkness

3: 24 h / 20 °C / Neat (no solvent)

4: water / 1 h

With sodium iodide; potassium hydroxide; In diethyl ether; water; acetone;

DOI:10.1002/jhet.876

Reference yield:

2-butylamino-ethanol (111-75-1) → N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium bis(trifluoromethanesulfonyl)imide (1391034-56-2)

Guidance literature:

Multi-step reaction with 4 steps

1: chlorosulfonic acid / 2 h / 0 - 150 °C

2: potassium hydroxide / water / 120 °C

3: 24 h / 20 °C / Neat (no solvent)

4: water / 1 h

With chlorosulfonic acid; potassium hydroxide; In water;

DOI:10.1002/jhet.876

upstream raw materials:

N-butylaziridine

2-(2-methoxyethoxy)ethyl iodide

N-butyl-N-[2-(2-methoxyethoxy)ethyl]aziridinium iodide

bis(trifluoromethane)sulfonimide lithium

Refernces