C₁₃H₇F₂NO₂

Base Information

• Chemical Name: C₁₃H₇F₂NO₂
• CAS No.: 1613479-45-0
• Molecular Formula: C₁₃H₇F₂NO₂
• Molecular Weight: 247.201
• Mol file: 1613479-45-0.mol

Synonyms:

Chemical Property of C₁₃H₇F₂NO₂

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₃H₇F₂NO₂

There total 2 articles about C₁₃H₇F₂NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

furo<2,3-c>pyridin-7(6H)-one (84400-98-6) → C13H7F2NO2 (1613479-45-0)

Guidance literature:

Multi-step reaction with 2 steps

1: trichlorophosphate / acetonitrile / 0.08 h / 110 °C / Microwave irradiation

2: sodium hydride / N,N-dimethyl acetamide; mineral oil / Inert atmosphere; Microwave irradiation

With sodium hydride; trichlorophosphate; In N,N-dimethyl acetamide; acetonitrile; mineral oil;

DOI:10.1016/j.bmcl.2014.04.045

Reference yield:

2,4-difluorophenol (367-27-1) + 7-Chlorofuro[2,3-c]pyridine (84400-99-7) → C13H7F2NO2 (1613479-45-0)

Guidance literature:

With sodium hydride; In N,N-dimethyl acetamide; mineral oil; Inert atmosphere; Microwave irradiation;

DOI:10.1016/j.bmcl.2014.04.045

upstream raw materials:

2,4-difluorophenol

7-Chlorofuro[2,3-c]pyridine

furo<2,3-c>pyridin-7(6H)-one

Refernces