CH₂CHCH₂P(OCH₃)2OBCl₂C₆H₁₁

Base Information

• Chemical Name: CH₂CHCH₂P(OCH₃)2OBCl₂C₆H₁₁
• CAS No.: 308795-33-7
• Molecular Formula: C₁₁H₂₂BCl₂O₃P
• Molecular Weight: 314.985
• Mol file: 308795-33-7.mol

Synonyms:

Chemical Property of CH₂CHCH₂P(OCH₃)2OBCl₂C₆H₁₁

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of CH₂CHCH₂P(OCH₃)2OBCl₂C₆H₁₁

There total 1 articles about CH₂CHCH₂P(OCH₃)2OBCl₂C₆H₁₁ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

allylphosphonic acid dimethyl ester (757-54-0) + (dichloro)(cyclohexyl)borane (39105-81-2) → CH2CHCH2P(OCH3)2OBCl2C6H11 (308795-33-7)

Guidance literature:

In toluene; neat phosphonate (1 equiv) was quickly added to a soln. of borane (1 equiv) in toluene at -30°C, the mixt. was warmed to ambient temp. (N2); not sepd., detected by NMR spectra;

DOI:10.1021/om000067v

Reference yield:

CH2CHCH2P(OCH3)2OBCl2C6H11 (308795-33-7) → (CH2CHCH2POCH3O2BClC6H11)2 (308795-37-1)

Guidance literature:

In ⁽²⁾H₈-toluene; the soln. was stored for 2 d at room temp. (N2 atm.);

DOI:10.1021/om000067v

Reference yield:

CH2CHCH2P(OCH3)2OBCl2C6H11 (308795-33-7) → allylphosphonic acid dimethyl ester (757-54-0) + cyclohexylboronic acid (4441-56-9)

Guidance literature:

In methanol; MeOH, 30°C (N2);

DOI:10.1021/om000067v

upstream raw materials:

allylphosphonic acid dimethyl ester

(dichloro)(cyclohexyl)borane

Downstream raw materials:

allylphosphonic acid dimethyl ester

cyclohexylboronic acid

(CH₂CHCH₂POCH₃O₂BClC₆H₁₁)2

Refernces