N-methyl-2-(2-methyl-benzyl)-aniline

Base Information

• Chemical Name: N-methyl-2-(2-methyl-benzyl)-aniline
• CAS No.: 408309-99-9
• Molecular Formula: C₁₅H₁₇N
• Molecular Weight: 211.307
• Mol file: 408309-99-9.mol

Synonyms:

Chemical Property of N-methyl-2-(2-methyl-benzyl)-aniline

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N-methyl-2-(2-methyl-benzyl)-aniline

There total 8 articles about N-methyl-2-(2-methyl-benzyl)-aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-Benzoylbenzoic acid (85-52-9) → N-methyl-2-(2-methyl-benzyl)-aniline (408309-99-9)

Guidance literature:

Multi-step reaction with 4 steps

1: nitric acid / Hydrieren des Reaktionsgemisches an Raney-Nickel in Methanol bei 40grad/85at und anschliessenden Erwaermen mit wss.Salzsaeure

2: copper oxide / chromium oxide; dioxane / 250 °C / 194910 Torr / Hydrogenation

3: diethyl ether / und Behandeln der Reaktionsloesung mit Methyljodid

4: potassium-sodium; 1,2-dimethoxy-ethane

With 1,4-dioxane; chromium(III) oxide; 1,2-dimethoxyethane; potassium Sodium; diethyl ether; nitric acid; copper(II) oxide;

Reference yield:

5,6-dihydro-6,11-dioxomorphanthridine (1143-50-6) → N-methyl-2-(2-methyl-benzyl)-aniline (408309-99-9)

Guidance literature:

Multi-step reaction with 3 steps

1: copper oxide / chromium oxide; dioxane / 250 °C / 194910 Torr / Hydrogenation

2: diethyl ether / und Behandeln der Reaktionsloesung mit Methyljodid

3: potassium-sodium; 1,2-dimethoxy-ethane

With 1,4-dioxane; chromium(III) oxide; 1,2-dimethoxyethane; potassium Sodium; diethyl ether; copper(II) oxide;

Reference yield:

5-methyl-6,11-dihydro-5H-dibenzo[b,e]azepine (1557-46-6) → N-methyl-2-(2-methyl-benzyl)-aniline (408309-99-9)

Guidance literature:

With 1,2-dimethoxyethane; potassium Sodium;

upstream raw materials:

5-methyl-6,11-dihydro-5H-dibenzo[b,e]azepine

2-Benzoylbenzoic acid

5,11-dihydro-6H-dibenz[b,e]azepin-6-one

5,6-dihydro-6,11-dioxomorphanthridine

Downstream raw materials:

N,N-dimethyl-2-(2-methyl-benzyl)-aniline