4,4'-Propane-1,1-diyldiphenol

Base Information

• Chemical Name: 4,4'-Propane-1,1-diyldiphenol
• CAS No.: 1576-13-2
• Molecular Formula: C15H16O2
• Molecular Weight: 228.291
• European Community (EC) Number: 635-810-9
• UNII: 21X1TQ2EMM
• DSSTox Substance ID: DTXSID3044594
• Nikkaji Number: J1.516.440I
• Wikidata: Q27148855
• Mol file: 1576-13-2.mol

Synonyms:4,4'-Propane-1,1-diyldiphenol;1576-13-2;4,4'-propylidenediphenol;4-[1-(4-hydroxyphenyl)propyl]phenol;1,1-Bis(4-hydroxyphenyl)propane;Phenol, 4,4'-propylidenebis-;21X1TQ2EMM;4,4'-propylidenebisphenol;UNII-21X1TQ2EMM;SCHEMBL74326;DTXSID3044594;CHEBI:79723;YKPAABNCNAGAAJ-UHFFFAOYSA-N;1,1-bis(4-hydroxyphenyl)-n-propane;AKOS024325181;Q27148855

Chemical Property of 4,4'-Propane-1,1-diyldiphenol

Chemical Property:

• XLogP3: 3.7
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 2
• Rotatable Bond Count: 3
• Exact Mass: 228.115029749
• Heavy Atom Count: 17
• Complexity: 191

Purity/Quality:

95% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Total 1 MSDS from other Authors

Useful:

• Canonical SMILES: CCC(C1=CC=C(C=C1)O)C2=CC=C(C=C2)O

Technology Process of 4,4'-Propane-1,1-diyldiphenol

There total 5 articles about 4,4'-Propane-1,1-diyldiphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

propionaldehyde (123-38-6) + phenol (108-95-2,27073-41-2) → 1,1-bis-(4-hydroxyphenyl)propane (1576-13-2)

Guidance literature:

With silica supported perchloric acid; In neat (no solvent); for 5.25h; Heating; Green chemistry;

DOI:10.1080/00304948.2020.1762459

Reference yield:

hydrogenchloride (7647-01-0,15364-23-5) + propionaldehyde (123-38-6) + phenol (108-95-2,27073-41-2) → 1,1-bis-(4-hydroxyphenyl)propane (1576-13-2)

Guidance literature:

analoge Reaktion mit o-Kresol, m-Kresol, Resorcin;

DOI:10.1021/ja01350a027

Reference yield:

diethylstilbesterol pinacolone (18922-13-9) → 1,1-bis-(4-hydroxyphenyl)propane (1576-13-2)

Guidance literature:

at 170 - 200 ℃;

DOI:10.1080/07315724.2002.10719192

upstream raw materials:

propionaldehyde

phenol

hydrogenchloride

diethylstilbesterol pinacolone

Downstream raw materials:

1,1-bis(4-methoxyphenyl)propane

4-n-Propylphenol

4-Propenyl-phenol

phenol

Refernces

• 1、 Gustafson, Jeffrey L.,Sigman, Matthew S.,Miller, Scott J.. "Linear free-energy relationship analysis of a catalytic desymmetrization reaction of a diarylmethane-bis(phenol)". supporting information; experimental part. p. 2794 - 2797. Retrieved 2010/09/04.
• 2、 -. "MANUFACTURING METHOD FOR POLYCARBONATE". . . Retrieved 2008/06/13.