triisopropoxy(1,3-dihydro-1,3-dioxo-α(benzyl)-2H-isoindole-2-acetato)zirconium (IV)

Base Information

• Chemical Name: triisopropoxy(1,3-dihydro-1,3-dioxo-α(benzyl)-2H-isoindole-2-acetato)zirconium (IV)
• CAS No.: 131135-98-3
• Molecular Formula: C₂₆H₃₃NO₇Zr
• Molecular Weight: 562.775
• Mol file: 131135-98-3.mol

Synonyms:

Chemical Property of triisopropoxy(1,3-dihydro-1,3-dioxo-α(benzyl)-2H-isoindole-2-acetato)zirconium (IV)

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of triisopropoxy(1,3-dihydro-1,3-dioxo-α(benzyl)-2H-isoindole-2-acetato)zirconium (IV)

There total 1 articles about triisopropoxy(1,3-dihydro-1,3-dioxo-α(benzyl)-2H-isoindole-2-acetato)zirconium (IV) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

zirconium(IV) tetraisopropoxide 2-propanol (14717-56-7) + N-phthaloylphenylalanine (3588-64-5) → triisopropoxy(1,3-dihydro-1,3-dioxo-α(benzyl)-2H-isoindole-2-acetato)zirconium (IV) (131135-98-3)

Guidance literature:

In benzene; byproducts: isopropanol; exclusion of moisture; molar ratio Zr(O-i-Pr)4*i-PrOH:ligand=1:1; refluxing; azeotropic removal of i-PrOH with benzene; removal of solvent in vac.; crystallization from benzene/hexane; elem. anal.;

upstream raw materials:

zirconium(IV) tetraisopropoxide 2-propanol

N-phthaloylphenylalanine

Refernces