Nsc81386

Base Information

• Chemical Name: Nsc81386
• CAS No.: 6002-83-1
• Molecular Formula: C17H18 N2 O4
• Molecular Weight: 314.341
• Mol file: 6002-83-1.mol

Synonyms:1,2-Hydrazinedicarboxylicacid, 1-methyl-, bis(phenylmethyl) ester (9CI); Bicarbamic acid, methyl-,dibenzyl ester (7CI,8CI); NSC 235821; NSC 81386

Chemical Property of Nsc81386

Chemical Property:

• PSA: 67.87000
• Density: 1.23g/cm³
• LogP: 3.48730

Purity/Quality:

≥95% ^*data from raw suppliers

DIBENZYL 1-METHYL-1,2-HYDRAZINEDICARBOXYLATE Aldrich ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Nsc81386

There total 2 articles about Nsc81386 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzyl chloroformate (501-53-1,94274-21-2) + methylhydrazine (60-34-4) → 1-methyl-1,2-dicarbobenzoxy-hydrazine (6002-83-1)

Guidance literature:

With sodium hydroxide;

Reference yield:

→ 1-methyl-1,2-dicarbobenzoxy-hydrazine (6002-83-1)

Guidance literature:

Methylhydrazin, Benzylchloroformat;

Reference yield: 97.0%

1-methyl-1,2-dicarbobenzoxy-hydrazine (6002-83-1) + 1-(2-chloroethyl)pyrrolidine hydrochloride (7250-67-1) → C23H29N3O4 (1609072-25-4)

Guidance literature:

1-methyl-1,2-dicarbobenzoxy-hydrazine; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Inert atmosphere;

1-(2-chloroethyl)pyrrolidine hydrochloride; With sodium iodide; In N,N-dimethyl-formamide; at 60 ℃; for 2h; Inert atmosphere;

upstream raw materials:

benzyl chloroformate

methylhydrazine

Downstream raw materials:

Bis(phenylmethyl)-1-(3-ethoxy-3-oxopropyl)-2-methyl-1,2-hydrazindicarboxylat

Bis(phenylmethyl)-1-(4-ethoxy-4-oxobutyl)-2-methyl-1,2-hydrazindicarboxylat

Bis(phenylmethyl)-1-(5-ethoxy-5-oxopentyl)-2-methyl-1,2-hydrazindicarboxylat

4-[(2-methyl-1,2-dicarbobenzoxy-hydrazino)-methyl]-benzoic acid

Refernces