2,4-DIHYDROXY-1,3,5-TRIMETHYLBENZENE

Base Information

• Chemical Name: 2,4-DIHYDROXY-1,3,5-TRIMETHYLBENZENE
• CAS No.: 608-98-0
• Molecular Formula: C9H12 O2
• Molecular Weight: 152.193
• Hs Code.: 2907299090
• Mol file: 608-98-0.mol

Synonyms:Mesorcinol(6CI); Resorcinol, 2,4,6-trimethyl- (7CI,8CI); 2,4-Mesitylenediol; Mesorcin;NSC 52676

Chemical Property of 2,4-DIHYDROXY-1,3,5-TRIMETHYLBENZENE

Chemical Property:

• Melting Point: 150.8°C
• Refractive Index: 1.4024 (estimate)
• Boiling Point: 274.5°C (estimate)
• PSA: 40.46000
• Density: 0.967g/cm³
• LogP: 2.02300

Purity/Quality:

98%min ^*data from raw suppliers

2,4-Dihydroxy-1,3,5-trimethylbenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2,4-DIHYDROXY-1,3,5-TRIMETHYLBENZENE

There total 15 articles about 2,4-DIHYDROXY-1,3,5-TRIMETHYLBENZENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,4-dinitromesitylene (608-50-4) → 2,4-dihydroxy-1,3,5-trimethylbenzene (608-98-0)

Guidance literature:

Multi-step reaction with 3 steps

1: aq. NH₃, H₂S / ethanol / Heating

2: (i) aq. H₂SO₄, NaNO₂, (ii) (heating)

3: (i) Sn, aq. HCl, (ii) NaNO₂, aq. H₂SO₄, (iii) (heating)

With ammonium hydroxide; hydrogen sulfide; In ethanol;

DOI:10.1139/v65-200

Reference yield:

1,3,5-trimethyl-benzene (108-67-8) → 2,4-dihydroxy-1,3,5-trimethylbenzene (608-98-0)

Guidance literature:

Multi-step reaction with 4 steps

1: HNO₃

2: aq. NH₃, H₂S / ethanol / Heating

3: (i) aq. H₂SO₄, NaNO₂, (ii) (heating)

4: (i) Sn, aq. HCl, (ii) NaNO₂, aq. H₂SO₄, (iii) (heating)

With ammonium hydroxide; hydrogen sulfide; nitric acid; In ethanol;

DOI:10.1139/v65-200

Reference yield:

6-acetoxy-2,4,6-trimethyl-cyclohexa-2,4-dienone (4906-82-5) → 2,4-dihydroxy-1,3,5-trimethylbenzene (608-98-0)

Guidance literature:

Multi-step reaction with 2 steps

1: H₂O / diethyl ether

2: aq. HCl / Heating

With hydrogenchloride; water; In diethyl ether;

DOI:10.1039/jr9600000001

upstream raw materials:

methanol

3,5-dihydroxyphenol

sodium methylate

4,6-Dimethoxy-2-hydroxy-3-methyl-isobutyrophenon

Refernces