α-(N-benzotriazol-2-yl)-p-phenylacetophenone phenylhydrazone

Base Information

• Chemical Name: α-(N-benzotriazol-2-yl)-p-phenylacetophenone phenylhydrazone
• CAS No.: 127876-46-4
• Molecular Formula: C₂₆H₂₁N₅
• Molecular Weight: 403.486
• Mol file: 127876-46-4.mol

Synonyms:

Chemical Property of α-(N-benzotriazol-2-yl)-p-phenylacetophenone phenylhydrazone

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of α-(N-benzotriazol-2-yl)-p-phenylacetophenone phenylhydrazone

There total 1 articles about α-(N-benzotriazol-2-yl)-p-phenylacetophenone phenylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium benzotriazolate (15217-42-2) + phenylhydrazine hydrochloride (59-88-1) + 2-Bromo-4'-phenylacetophenone (135-73-9) → α-(N-benzotriazol-2-yl)-p-phenylacetophenone phenylhydrazone (127876-46-4) + α-(N-benzotriazol-1-yl)-p-phenylacetophenone phenylhydrazone (127876-45-3)

Guidance literature:

With pyridine; Multistep reaction. Title compound not separated from byproducts; 1.) THF, heating, 1 h, 2.) ethanol, reflux, 30 min;

upstream raw materials:

sodium benzotriazolate

phenylhydrazine hydrochloride

2-Bromo-4'-phenylacetophenone

Refernces