sodium 2-(acetylamino)benzoate

Base Information

• Chemical Name: sodium 2-(acetylamino)benzoate
• CAS No.: 2870-60-2
• Molecular Formula: C9H9NO3.Na
• Molecular Weight: 201.157
• Mol file: 2870-60-2.mol

Synonyms:EINECS 220-699-8;ortho-acetamidobenzoate;2-acetylamino-benzoic acid,sodium salt;sodium 2-acetamidobenzoate;

Chemical Property of sodium 2-(acetylamino)benzoate

Chemical Property:

• Vapor Pressure: 6.67E-08mmHg at 25°C
• Boiling Point: 422.8oC at 760 mmHg
• Flash Point: 209.5oC
• PSA: 72.72000
• LogP: 1.86520

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium 2-(acetylamino)benzoate

There total 1 articles about sodium 2-(acetylamino)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

sodium o-aminobenzoate (552-37-4) + acetic anhydride (108-24-7) → sodium 2-(acetylamino)benzoate (2870-60-2)

Guidance literature:

In water;

DOI:10.1016/j.tetlet.2003.11.111

Reference yield: 77.0%

sodium 2-(acetylamino)benzoate (2870-60-2) + allyl bromide (106-95-6) → allyl o-acetamidobenzoate (82679-10-5)

Guidance literature:

In dimethyl sulfoxide; at 65 ℃; for 5h;

DOI:10.1016/j.tetlet.2003.11.111

Reference yield: 42.0%

bis(cyclopentadienyl)titanium dichloride (1271-19-8) + sodium 2-(acetylamino)benzoate (2870-60-2) → (C5H5)2Ti(CH3CONHC6H4CO2)2 (108456-50-4)

Guidance literature:

In benzene; mixt. of complex and Na-salt of benzoic acid in dry benzene was stirredfor 3-8 h at 30°C; filtered, filtrate was evapd., recrystd. from boiling benzene; elem. anal.;

upstream raw materials:

sodium o-aminobenzoate

acetic anhydride

Downstream raw materials:

2-acetylamino-benzoic acid 2-morpholin-4-yl-ethyl ester

2-amino-benzoic acid 2-(2-morpholin-4-yl-ethoxy)-ethyl ester

allyl o-acetamidobenzoate

(C₅H₅)2Ti(CH₃CONHC₆H₄CO₂)2

Refernces