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1021949-47-2

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Basic Information
CAS No.: 1021949-47-2
Name: 5-[1-(2,3-DiMethylphenyl)ethenyl]iMidazole
Article Data: 7
Molecular Structure:
Molecular Structure of 1021949-47-2 (5-[1-(2,3-DiMethylphenyl)ethenyl]iMidazole)
Formula: C13H14N2
Molecular Weight: 198.268
Synonyms: 5-[1-(2,3-dimethylphenyl)ethenyl]-1H-imidazole
Density: 1.066
Boiling Point: 393.2±11.0 °C(Predicted)
PSA: 28.68000
LogP: 3.08800
Related products
Synthetic route

1-(2,3-dimethylphenyl)-1-(1H-imidazol-4-yl)ethanol

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
With toluene-4-sulfonic acid In toluene at 0.11℃; for 2h; Reagent/catalyst; Solvent; Temperature; Dean-Stark;100%

4-(2,3-dimethylbenzoyl)-1H-imidazole

1779-49-3

Methyltriphenylphosphonium bromide

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
With potassium tert-butylate In tetrahydrofuran at 20 - 25℃; for 18h; Wittig Olefination;94%

(1-trityl-1H-imidazol-4-yl)boronic acid

C10H11Br

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
Stage #1: (1-trityl-1H-imidazol-4-yl)boronic acid; C10H11Br With tris-(dibenzylideneacetone)dipalladium(0); sodium phosphate In 5,5-dimethyl-1,3-cyclohexadiene; water at 105℃; Inert atmosphere;
Stage #2: With toluene-4-sulfonic acid In tetrahydrofuran at 20 - 65℃; for 1.5h; Reagent/catalyst; Solvent; Temperature;		74.9%

5-[1-(2,3-dimethylphenyl)vinyl]-1H-imidazole hydrochloride

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
With sodium hydroxide; water at 0 - 25℃; for 1 - 1.5h;
176721-02-1

4-<(2,3-dimethylphenyl)carbonyl>-1-(triphenylmethyl)imidazole

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
1.2: 24 h / 0 °C / Inert atmosphere
2.1: trifluoroacetic acid; water / 12 h / 20 °C
View Scheme
Multi-step reaction with 2 steps
1.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C
1.2: 4 h / 20 °C
2.1: hydrogenchloride / dichloromethane
View Scheme

4-(1-(2,3-dimethylphenyl)vinyl)-1-trityl-1H-imidazole

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
With water; trifluoroacetic acid at 20℃; for 12h;
With hydrogenchloride In dichloromethane19.5 g
176721-01-0

4-<(2,3-dimethylphenyl)hydroxymethyl>-1-(triphenylmethyl)imidazole

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: manganese(IV) oxide / 1,4-dioxane / Reflux
2.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
2.2: 24 h / 0 °C / Inert atmosphere
3.1: trifluoroacetic acid; water / 12 h / 20 °C
View Scheme
Multi-step reaction with 3 steps
1: manganese(IV) oxide / 1,4-dioxane / 5 h / Reflux
2: tetrahydrofuran; diethyl ether / 2 h / 0 - 20 °C
3: triethylsilane; trifluoroacetic acid / dichloromethane / 4 h / -10 °C
View Scheme
Multi-step reaction with 3 steps
1.1: manganese(IV) oxide / 1,4-dioxane / 3 h / Reflux
2.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C
2.2: 4 h / 20 °C
3.1: hydrogenchloride / dichloromethane
View Scheme
576-23-8

2,3-dimethylbromobenzene

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: magnesium / tetrahydrofuran
1.2: 0 °C
2.1: manganese(IV) oxide / 1,4-dioxane / Reflux
3.1: n-butyllithium / hexane; tetrahydrofuran / 1 h / 0 °C / Inert atmosphere
3.2: 24 h / 0 °C / Inert atmosphere
4.1: trifluoroacetic acid; water / 12 h / 20 °C
View Scheme
Multi-step reaction with 4 steps
1.1: magnesium; iodine / tetrahydrofuran / 1 h / Reflux
1.2: 1.5 h / 0 - 20 °C
2.1: manganese(IV) oxide / 1,4-dioxane / 5 h / Reflux
3.1: tetrahydrofuran; diethyl ether / 2 h / 0 - 20 °C
4.1: triethylsilane; trifluoroacetic acid / dichloromethane / 4 h / -10 °C
View Scheme
Multi-step reaction with 4 steps
1.1: (bis(tricyclohexyl)phosphine)palladium(II) dichloride; copper(l) iodide; N-ethyl-N,N-diisopropylamine / 2-methyltetrahydrofuran / 30 °C / Inert atmosphere
2.1: caesium carbonate / ethanol / 30 °C / Inert atmosphere
3.1: hydrogen bromide; acetic acid / dichloromethane / 0 - 10 °C / Inert atmosphere
4.1: sodium phosphate; tris-(dibenzylideneacetone)dipalladium(0) / 5,5-dimethyl-1,3-cyclohexadiene; water / 105 °C / Inert atmosphere
4.2: 1.5 h / 20 - 65 °C
View Scheme
Multi-step reaction with 4 steps
1.1: magnesium; iodine / tetrahydrofuran / 1.5 h / 70 °C / Inert atmosphere
1.2: -5 - 20 °C / Inert atmosphere
2.1: manganese(IV) oxide / 1,4-dioxane / 3 h / Reflux
3.1: potassium tert-butylate / tetrahydrofuran / 0.5 h / 0 °C
3.2: 4 h / 20 °C
4.1: hydrogenchloride / dichloromethane
View Scheme
Multi-step reaction with 3 steps
1.1: ethylene dibromide; magnesium / tetrahydrofuran / 1 h / 40 - 65 °C
1.2: 2 h / -5 - 0 °C
1.3: 3 h / 30 °C
2.1: tetrahydrofuran / 2 h / 0.4 - 65 °C / Large scale
3.1: toluene-4-sulfonic acid / toluene / 2 h / 0.11 °C / Dean-Stark
View Scheme

(2,3-dimethylphenyl)(1H-imidazol-4-yl)methanol

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Dess-Martin periodane; magnesium sulfate / dichloromethane / 12 h / 20 - 30 °C
2: potassium tert-butylate / tetrahydrofuran / 18 h / 20 - 25 °C
View Scheme
5779-93-1

2,3-dimethylbenzaldehyde

1021949-47-2

1-(4-imidazolyl)-1-(2,3-dimethylphenyl)ethylene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: magnesium; iodine / tetrahydrofuran / 35 - 65 °C / Inert atmosphere
1.2: 6 h / 20 - 25 °C
2.1: Dess-Martin periodane; magnesium sulfate / dichloromethane / 12 h / 20 - 30 °C
3.1: potassium tert-butylate / tetrahydrofuran / 18 h / 20 - 25 °C
View Scheme
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  • 5-[1-(2,3-Dimethylphenyl)ethenyl]-1H-imidazole CAS NO.1021949-47-2

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    1021949-47-2

    5-[1-(2,3-Dimethylphenyl)ethenyl]-1H-imidazole CAS NO.1021949-47-2

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    1021949-47-2

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    1021949-47-2

    5-[1-(2,3-Dimethylphenyl)vinyl]-1H-imidazole

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  • 5-[1-(2,3-Dimethylphenyl)ethenyl]-1H-imidazole

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    1021949-47-2

    5-[1-(2,3-Dimethylphenyl)ethenyl]-1H-imidazole

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    1021949-47-2

    5-[1-(2,3-Dimethylphenyl)ethenyl]-1H-imidazole

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    1021949-47-2

    5-[1-(2,3-DiMethylphenyl)ethenyl]iMidazole

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    1021949-47-2

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    1021949-47-2

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    1021949-47-2

    Medetomidine Impurity 3

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    1021949-47-2

    5-(1-(2,3-dimethylphenyl)vinyl)-1H-imidazole

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    We are a leading global supplier and manufacturer of chiral chemicals, amino acids, aromatic and pyridine halogens, natural extracts and pharmaceutical raw materials. Those chemica

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    1021949-47-2

    Medetomidine Impurity 3

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