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111324-04-0

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CAS No.: 111324-04-0
Name: 1-TERT-BUTYL-4,4,4-TRIS(DIMETHYLAMINO)-2,2-BIS[TRIS(DIMETHYLAMINO)-PHOSPHORANYLIDE-NAMINO]-2LAMBDA5,4LAMBDA5-CATENADI(PHOSPHAZENE)
Article Data: 2
Molecular Structure:
Molecular Structure of 111324-04-0 (1-TERT-BUTYL-4,4,4-TRIS(DIMETHYLAMINO)-2,2-BIS[TRIS(DIMETHYLAMINO)-PHOSPHORANYLIDE-NAMINO]-2LAMBDA5,4LAMBDA5-CATENADI(PHOSPHAZENE))
Formula: C22H63 N13 P4
Molecular Weight: 633.724
Synonyms: Phosphorimidictriamide, (1,1-dimethylethyl)tris[tris(dimethylamino)phosphoranylidene]- (9CI);(tert-Butylimino)tris((tris(dimethylamino)phosphoranylidene)amino)phosphorane;1-Tert-butyl-4,4,4-tris(dimethylamino)-2,2-bis[tris(dimethylamino)phosphoranylideneamino]-2l5,4l5-catenadi(phosphazene); 3-(tert-Butylimino)-1,1,1,5,5,5-hexakis(dimethylamino)-3-[[tris(dimethylamino)phosphoranylidene]amino]-1l5,3l5,5l5-1,4-triphosphazadiene; Schwesinger P4 base; tert-Butyltris[tris(dimethylamino)phosphoranylidene]phosphorimidic triamide
Density: 0.90 g/mL at 20 °C
Melting Point: 207°
Boiling Point: 608.0±38.0 °C(Predicted)
Flash Point: -26 °C
Hazard Symbols:
Risk Codes: 11-34-48/20-51/53-62-65-67
Safety:
Hazard Codes F,C,N
Risk Statements 11-34-48/20-51/53-62-65-67
Safety Statements 26-36/37/39-45-61-62
RIDADR UN 2924 3/PG 2
WGK Germany 3
F 3-10-34
HazardClass 8
PackingGroup I
PSA: 117.84000
LogP: 5.62410
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111324-04-0

phosphazene base-P4-tert-butyl

Conditions
ConditionsYield
Yield given. Multistep reaction;
...Expand
111324-04-0

phosphazene base-P4-tert-butyl

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trifluoroacetic acid

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Conditions
ConditionsYield
In tetrahydrofuran for 2h;100%
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4,4-bis(4-hydroxyphenyl)valeric acid

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phosphazene base-P4-tert-butyl

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Conditions
ConditionsYield
In tetrahydrofuran; hexane at 20℃; for 12h; Inert atmosphere;95%
2683-82-1

2,3,7,8,12,13,17,18-octaethyl-porphyrin

111324-04-0

phosphazene base-P4-tert-butyl

C36H45N4(1-)*C22H64N13P4(1+)

Conditions
ConditionsYield
In tetrahydrofuran Ambient temperature; equilibrium;85%
75-46-7

trifluoromethan

124-38-9

carbon dioxide

111324-04-0

phosphazene base-P4-tert-butyl

C2HF3O2*C22H63N13P4

Conditions
ConditionsYield
In tetrahydrofuran; hexane at -40℃; for 24h; Inert atmosphere;78%
...Expand

hydroxygallium naphthalocyaninetetrasulfonic acid

111324-04-0

phosphazene base-P4-tert-butyl

4C22H63N13P4*C48H25GaN8O13S4

Conditions
ConditionsYield
In methanol; hexane75%
111324-04-0

phosphazene base-P4-tert-butyl

C22H63CaI2N13P4

Conditions
ConditionsYield
With N,N,N,N,-tetramethylethylenediamine; calcium iodide In benzene at 80℃; for 2h;34%
111324-04-0

phosphazene base-P4-tert-butyl

1315316-97-2

1-tert-butyl-4,4,4-tris(dimethylamino)-2,2-bis[tris(dimethylamino)phosphoranylidenamino]-2λ5,4λ5-catenadiphosphazenium fluoride

Conditions
ConditionsYield
With triethylamine hydrofluoride In diethyl ether for 1h; Inert atmosphere;31%
111-83-1

1-bromo-octane

111324-04-0

phosphazene base-P4-tert-butyl

A

3-(tert-Butylamino)-1,1,1,5,5,5-hexakis(dimethylamino)-3-[(tris(dimethylamino)phosphoranylidene)amino]-1λ5,5λ5-triphosphazadiene-3-ium bromide

B

C30H80N13P4(1+)*Br(1-)

Conditions
ConditionsYield
In tetrahydrofuran; xylene for 6h; Ambient temperature; Title compound not separated from byproducts;
...Expand
111324-04-0

phosphazene base-P4-tert-butyl

74-88-4

methyl iodide

A

P4-tBu*BF4

B

3-(tert-Butylmethylamino)-1,1,1,5,5,5-hexakis(dimethylamino)-3-[(tris(dimethylamino)phosphoranylidene)amino]-1λ5,5λ5-triphosphazadien-3-ium tetrafluoroborate

Conditions
ConditionsYield
With sodium tetrafluoroborate 1.) THF, r.t., overnight, 2.) CH2Cl2; Multistep reaction. Title compound not separated from byproducts;
...Expand
Raw Materials
124-40-3
49778-01-0
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