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120739-62-0

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CAS No.: 120739-62-0
Name: N-[(6-CHLOROPYRIDIN-3-YL)METHYL]-N-METHYLAMINE
Article Data: 14
Molecular Structure:
Molecular Structure of 120739-62-0 (N-[(6-CHLOROPYRIDIN-3-YL)METHYL]-N-METHYLAMINE)
Formula: C7H9ClN2
Molecular Weight: 156.615
Synonyms: N-[(6-CHLOROPYRIDIN-3-YL)METHYL]-N-METHYLAMINE;2-CHLORO-5-(METHYLAMINOMETHYL)PYRIDINE;[(6-chloropyridin-3-yl)methyl]methylamine dihydrochloride;1-(6-chloropyridin-3-yl)-N-methylmethanamine;1-(6-chloro-3-pyridinyl)-N-methylmethanamine(SALTDATA: 1.4 HCl);1-(6-chloro-3-pyridinyl)-N-methylmethanamine 1.4 HCl;1-(6-Chloropyridin-3-yl)-N-MethylMethanaMine dihydrochloride;N-[(6-Chloropyridin-3-yl)methyl]methylamine
Density: 1.149±0.06 g/cm3(Predicted)
Boiling Point: 236.9±25.0 °C(Predicted)
PSA: 24.92000
LogP: 1.84530
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Synthetic route
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Conditions
ConditionsYield
Stage #1: methylamine In toluene at -5 - 5℃; Large scale;
Stage #2: 2-chloro-5-(chloromethyl)pyridine In toluene at -5 - 2℃; Large scale;		98.5%
In water at 62℃; under 1650.17 Torr; for 1h; Temperature; Pressure;97.7%
In water at 60℃; for 6h;95.6%
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1-(6-chloropyridin-3-yl)-N-methylmethanamine

Conditions
ConditionsYield
With methylamine In ethanol; water
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dimethyl sulfate

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Conditions
ConditionsYield
With sodium hydroxide; formic acid In water; toluene
...Expand
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2-chloro-5-(Trichloromethyl)-pyridine

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1-(6-chloropyridin-3-yl)-N-methylmethanamine

Conditions
ConditionsYield
With sodium hydroxide; methylamine; aluminum nickel In ethanol; water
With methylamine; aluminum nickel In ethanol; toluene
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(E) N'-carbamoyl-N[(6-chloropyridin-3-yl)methyl]-N-methylacetimidamide

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Conditions
ConditionsYield
In aq. phosphate buffer at 30℃; for 96h; Time;
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Conditions
ConditionsYield
In ethanol at 80℃;98%

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Conditions
ConditionsYield
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 2h;97.8%
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ethyl N-cyanoacetoimidate

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acetamiprid

Conditions
ConditionsYield
In ethanol at 65℃;96.6%
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ethyl N‐cyanoethanimidate

120739-62-0

1-(6-chloropyridin-3-yl)-N-methylmethanamine

acetamiprid

Conditions
ConditionsYield
at 75℃; for 9h; Industrial scale;96%

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6-chloro-N-[2-methyl-4-(3-trifluoromethoxyphenyl)-butyl]-N-methyl-pyridin-3-ylmethylamine

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ConditionsYield
With sodium tris(acetoxy)borohydride In 1,2-dichloro-ethane at 20℃; for 2.5h;92.3%
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