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122455-84-9

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Basic Information
CAS No.: 122455-84-9
Name: 4-FLUORO-6-METHYL-3-NITROPHENOL
Article Data: 13
Molecular Structure:
Molecular Structure of 122455-84-9 (4-FLUORO-6-METHYL-3-NITROPHENOL)
Formula: C7H6 F N O3
Molecular Weight: 171.128
Synonyms: 2-Methyl-4-fluoro-5-nitrophenol;4-Fluoro-2-methyl-5-nitrophenol
Density: 1.423g/cm3
Melting Point: 138-142 °C
Boiling Point: 325.1°Cat760mmHg
Flash Point: 150.4°C
PSA: 66.05000
LogP: 2.27110
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122455-84-9

2-methyl-4-fluoro-5-nitrophenol

Conditions
ConditionsYield
With ammonia In water at 20℃; for 1h;100%
With water; sodium hydroxide for 2h; Reflux;93%
With boron tribromide In dichloromethane at 0 - 20℃; for 18h;85%
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(4-fluoro-2-methylphenyl)methylcarbonate

122455-84-9

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Conditions
ConditionsYield
With sulfuric acid; nitric acid at 50℃; for 2h; Nitration; Deacetylation;22%
With nitric acid In sulfuric acid; water22%
With nitric acid In sulfuric acid; water22%

122455-84-9

2-methyl-4-fluoro-5-nitrophenol

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 86 percent / pyridine / dioxane / 0 - 20 °C
2: 90 percent / HNO3; H2SO4 / 0.5 h / 0 °C
3: 85 percent / BBr3 / CH2Cl2 / 18 h / 0 - 20 °C
View Scheme
Multi-step reaction with 2 steps
1: 78 percent / aq. NaOH / 2 h / 0 °C
2: 22 percent / HNO3; H2SO4 / 2 h / 50 °C
View Scheme
122455-84-9

2-methyl-4-fluoro-5-nitrophenol

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1-fluoro-4-methoxy-5-methyl-2-nitro-benzene

Conditions
ConditionsYield
With sodium carbonate In acetone at 20℃;100%
With sodium carbonate In acetone at 20℃;100%
With potassium carbonate In N,N-dimethyl-formamide at 20℃; for 1.5h;93%
100-39-0

benzyl bromide

122455-84-9

2-methyl-4-fluoro-5-nitrophenol

5-benzyloxy-2-fluoro-4-methyl-1-nitrobenzene

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide89%
With potassium carbonate In DMF (N,N-dimethyl-formamide) at 80℃; for 4h;89%
122455-84-9

2-methyl-4-fluoro-5-nitrophenol

4163-65-9

per-O-acetyl-α-D-mannopyranose

4-fluoro-2-methyl-5-nitrophenyl 2,3,4,6-tetra-O-acetyl-α-D-mannopyranoside

Conditions
ConditionsYield
With boron trifluoride diethyl etherate; triethylamine In dichloromethane at 40℃; for 48.5h; Inert atmosphere;88%
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isopropyl alcohol

122455-84-9

2-methyl-4-fluoro-5-nitrophenol

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4-fluoro-2-methyl-5-nitrophenyl 1-methylethyl ether

Conditions
ConditionsYield
Stage #1: isopropyl alcohol; 2-methyl-4-fluoro-5-nitrophenol With 2-(diphenylphosphino)pyridine; di-tert-butyl-diazodicarboxylate In tetrahydrofuran at 20℃; for 3h;
Stage #2: With hydrogenchloride In tetrahydrofuran; diethyl ether for 1h;		63%
122455-84-9

2-methyl-4-fluoro-5-nitrophenol

122455-85-0

2-fluoro-5-hydroxy-4-methylaniline

Conditions
ConditionsYield
With hydrogen; palladium 10% on activated carbon In methanol under 1551.49 Torr; for 2h;62%
With iron; iron(II) sulfate In water for 4h; Reduction; Heating;47%
With iron; iron(II) sulfate In water for 4h; Heating / reflux;47%
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2-methyl-4-fluoro-5-nitrophenol

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6-cyano-4-(2-fluoro-5-hydroxy-4-methylanilino)-7-(2-methoxyethoxy)quinoline hydrochloride

Conditions
ConditionsYield
With iron; iron(II) sulfate In water for 4h; Heating / reflux;47%
7439-89-6

iron

iron(II) sulfate

122455-84-9

2-methyl-4-fluoro-5-nitrophenol

122455-85-0

2-fluoro-5-hydroxy-4-methylaniline

Conditions
ConditionsYield
In water47%
In water47%
In water47%
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