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126257-22-5

Basic Information
CAS No.: 126257-22-5
Name: 1-(9-anthracenylmethyl)piperazine
Article Data: 5
Molecular Structure:
Molecular Structure of 126257-22-5 (1-(9-anthracenylmethyl)piperazine)
Formula: C19H20N2
Molecular Weight: 276.381
Density: 1.151±0.06 g/cm3(Predicted)
Boiling Point: 464.0±25.0 °C(Predicted)
PSA: 15.27000
LogP: 3.66490
Synthetic route
1419212-75-1

4-anthracen-9-ylmethylpiperazine-1-carboxylic acid tert-butyl ester

126257-22-5

9-(1',4'-diazacyclohexyl)methylanthracene

Conditions
ConditionsYield
With trifluoroacetic acid In dichloromethane at 20℃; for 2h;93%
With hydrogenchloride In methanol; water at 20℃; for 1h; Inert atmosphere;70%
110-85-0

piperazine

24463-19-2

anthracenylmethyl chloride

126257-22-5

9-(1',4'-diazacyclohexyl)methylanthracene

Conditions
ConditionsYield
In toluene for 6h; Heating;
24463-19-2

anthracenylmethyl chloride

A

4-(4'-(9''-anthrylmethyl)-1'-piperazino)phenylsulfonium hexafluorophosphate

4-(4'-(9''-anthrylmethyl)-1'-piperazino)phenylsulfonium hexafluorophosphate

B

126257-22-5

9-(1',4'-diazacyclohexyl)methylanthracene

Conditions
ConditionsYield
In piperazine
24463-19-2

anthracenylmethyl chloride

126257-22-5

9-(1',4'-diazacyclohexyl)methylanthracene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: potassium carbonate / acetonitrile / 18 h / Reflux; Inert atmosphere
2: hydrogenchloride / water; methanol / 1 h / 20 °C / Inert atmosphere
View Scheme
Multi-step reaction with 2 steps
1: potassium carbonate / acetonitrile / 60 °C
2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C
View Scheme
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    1-(9-anthracenylmethyl)piperazine CAS 126257-22-5

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