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CAS No.: | 126257-22-5 |
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Name: | 1-(9-anthracenylmethyl)piperazine |
Article Data: | 5 |
Molecular Structure: | |
Formula: | C19H20N2 |
Molecular Weight: | 276.381 |
Density: | 1.151±0.06 g/cm3(Predicted) |
Boiling Point: | 464.0±25.0 °C(Predicted) |
PSA: | 15.27000 |
LogP: | 3.66490 |
4-anthracen-9-ylmethylpiperazine-1-carboxylic acid tert-butyl ester
9-(1',4'-diazacyclohexyl)methylanthracene
Conditions | Yield |
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With trifluoroacetic acid In dichloromethane at 20℃; for 2h; | 93% |
With hydrogenchloride In methanol; water at 20℃; for 1h; Inert atmosphere; | 70% |
piperazine
anthracenylmethyl chloride
9-(1',4'-diazacyclohexyl)methylanthracene
Conditions | Yield |
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In toluene for 6h; Heating; |
Conditions | Yield |
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In piperazine |
anthracenylmethyl chloride
9-(1',4'-diazacyclohexyl)methylanthracene
Conditions | Yield |
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Multi-step reaction with 2 steps 1: potassium carbonate / acetonitrile / 18 h / Reflux; Inert atmosphere 2: hydrogenchloride / water; methanol / 1 h / 20 °C / Inert atmosphere View Scheme | |
Multi-step reaction with 2 steps 1: potassium carbonate / acetonitrile / 60 °C 2: trifluoroacetic acid / dichloromethane / 2 h / 20 °C View Scheme |