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129228-07-5

Basic Information
CAS No.: 129228-07-5
Name: Heptane, 4,4-bis(methoxymethyl)-2,6-dimethyl-
Article Data: 1
Molecular Structure:
Molecular Structure of 129228-07-5 (Heptane, 4,4-bis(methoxymethyl)-2,6-dimethyl-)
Formula: C13H28O2
Molecular Weight: 216.364
Synonyms: 2,2-di-i-butyl-1,3-dimethoxypropane;
Density: 0.843±0.06 g/cm3(Predicted)
Boiling Point: 203.1±8.0 °C(Predicted)
PSA: 18.46000
LogP: 3.35780
Synthetic route
129228-07-5

2,2-di-i-butyl-1,3-dimethoxypropane

7550-45-0

titanium tetrachloride

μ-oxo-bis{trichloro(2,2-diisobutyl-1,3-dimethoxypropane-O,O')titanium(IV)}

Conditions
ConditionsYield
With air; water In n-heptane reaction of TiCl4 and the ligand in n-heptane gives the monomeric intermediate which is converted to the product by standing in moist air;
129228-07-5

2,2-di-i-butyl-1,3-dimethoxypropane

2414-98-4

magnesium ethylate

7550-45-0

titanium tetrachloride

solid catalyst component

solid catalyst component

Conditions
ConditionsYield
Stage #1: magnesium ethylate; titanium tetrachloride In toluene at 5℃; for 1h;
Stage #2: 2,2-di-i-butyl-1,3-dimethoxypropane In toluene at 100℃; for 2h;
Stage #3: titanium tetrachloride In toluene at 110℃; for 2h;
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