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Basic Information
| CAS No.: | 14717-56-7 | ||||||||||||||
|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|---|
| Name: | ZIRCONIUM(IV) ISOPROPOXIDE ISOPROPANOL | ||||||||||||||
| Article Data: | 5 | ||||||||||||||
| Molecular Structure: | |||||||||||||||
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| Formula: | C15H36 O5 Zr | ||||||||||||||
| Molecular Weight: | 387.672 | ||||||||||||||
| Synonyms: | Zirconiumisopropoxide, compd. with iso-PrOH (1:1) (6CI); Zirconium,tetraisopropoxy(isopropyl alcohol)- (8CI); 2-Propanol, zirconium complex;Isopropyl alcohol, compd. with zirconium isopropoxide (1:1) (8CI);(Isopropanol)tetrakis(isopropoxo)zirconium;Isopropanoltetrakis(isopropanolato)zirconium | ||||||||||||||
| Hazard Symbols: |
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| Risk Codes: | 36/37/38 | ||||||||||||||
| Safety: |
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| PSA: | 57.15000 | ||||||||||||||
| LogP: | 3.88990 | ||||||||||||||
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Synthetic route
- 10026-11-6
zirconium(IV) chloride
- 67-63-0
isopropyl alcohol
- 14717-56-7
zirconium(IV) tetraisopropoxide 2-propanol
Conditions
| Conditions | Yield |
|---|---|
| In not given N2 atmosphere; |
Conditions
| Conditions | Yield |
|---|---|
| In isopropyl alcohol according Shreider, Turevskaya, Kozlova, Turova; Izv. Akad. Nauk SSR. Ser. Khim., No.8, 1687-1692 (1981);; recrystd. in i-PrOH;;; | |
| In not given Electrolysis; Zr anode, Zr cathode, Ar-atmosphere, stirring, 110 V/0.23 A, 15 h; soln.contg. various salts (Bu4NBr, Bu4NBF4, NaBr or other); crystn. on cooling; elem. anal.; | |
| With Bu4NBr In neat (no solvent) byproducts: H2; Electrochem. Process; Ar, at 110 V for 15 h; recrystd. from alcohol; elem. anal.; | |
| With LiCl In isopropyl alcohol Electrochem. Process; anodic dissoln. in anhyd. alcohol (supporting electrolyte LiCl), according to: V. A. Shreider, E. P. Turevskaya, N. I. Kozlova, N. Ya. Turova, Inorg. Chim. Acta 53 (1981) 73; recrystn. (isopropanol); |
- 586-98-1
2-Hydroxymethylpyridine
- 14717-56-7
zirconium(IV) tetraisopropoxide 2-propanol
- 1346523-15-6
C18H26N2O4Zr
Conditions
| Conditions | Yield |
|---|---|
| In cyclohexane at 20℃; Schlenk technique; Inert atmosphere; | 100% |
- 14717-56-7
zirconium(IV) tetraisopropoxide 2-propanol
- 18166-43-3
tris(tert-butoxy)silanol
- 1392309-85-1
[Zr(O-i-Pr)3(OSi(O-t-Bu)3)]
Conditions
| Conditions | Yield |
|---|---|
| In benzene soln. (HOSi(O-t-Bu)3) in benzene was added to soln.(Zr(O-i-Pr)4*i-PrOH) in benzene (1:1), refluxed for 4 h; react. mixt. was concd. in vacuo; elem. anal.; | 99% |
- 14717-56-7
zirconium(IV) tetraisopropoxide 2-propanol
- 18166-43-3
tris(tert-butoxy)silanol
- 36809-78-6
[Zr(O-i-Pr)2(OSi(O-t-Bu)3)2]
Conditions
| Conditions | Yield |
|---|---|
| In benzene soln. (HOSi(O-t-Bu)3) in benzene was added to soln.(Zr(O-i-Pr)4*i-PrOH) in benzene (2:1), refluxed for 8 h; react. mixt. was concd. in vacuo; elem. anal.; | 99% |
Conditions
| Conditions | Yield |
|---|---|
| In diethyl ether at -35 - 20℃; for 2h; Inert atmosphere; Schlenk technique; Glovebox; | 99% |
Conditions
| Conditions | Yield |
|---|---|
| In diethyl ether at -35 - 0℃; for 2h; Inert atmosphere; Glovebox; Schlenk technique; | 99% |
- 14717-56-7
zirconium(IV) tetraisopropoxide 2-propanol
- 1070655-38-7
Hf(OiPr)4·HOiPr
- 1443147-87-2
C42H74HfNO5
Conditions
| Conditions | Yield |
|---|---|
| In diethyl ether at -35 - 0℃; for 4h; Inert atmosphere; Glovebox; Schlenk technique; | 99% |
- 14717-56-7
zirconium(IV) tetraisopropoxide 2-propanol
- 102-71-6
triethanolamine
- 151767-62-3
zirconium bis(triethanolaminate)
Conditions
| Conditions | Yield |
|---|---|
| In benzene byproducts: i-PrOH; 2 equiv. of triethanolamine was added to C6H6 soln. of Zr-complex, reflux for 12 h with recovering of i-PrOH as azeotrope; mixt. was allowed to stand to room temp., volatiles were removed in vac., elem. anal.; | 97% |
- 14717-56-7
zirconium(IV) tetraisopropoxide 2-propanol
- 444777-27-9
furan-2-carboxylic acid
Conditions
| Conditions | Yield |
|---|---|
| In benzene byproducts: iPrOH; to soln. of Zr compd. ligand added (1:3), refluxed for 8 h; stood, washed with EtOH, dried (E-2 torr, 4 h); elem. anal.; | 96% |
Raw Materials
Downstream Products
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ZIRCONIUM(IV) ISOPROPOXIDE ISOPROPANOL
