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15520-05-5

Basic Information
CAS No.: 15520-05-5
Name: 2,2'-(octylimino)bisethanol
Article Data: 10
Molecular Structure:
Molecular Structure of 15520-05-5 (2,2'-(octylimino)bisethanol)
Formula: C12H27 N O2
Molecular Weight: 217.352
Synonyms: Ethanol,2,2'-(octylimino)di- (8CI); 2,2'-(Octylimino)diethanol;Bis(2-hydroxyethyl)octylamine; Diethanoloctylamine; Hetoxamine OT 2;N,N-Bis(2-hydroxyethyl)octylamine; N-Octyldiethanolamine; Octyldiethanolamine
Density: 0.949g/cm3
Boiling Point: 342.4°Cat760mmHg
Flash Point: 150.5°C
Solubility: 1.4g/L at 20℃
PSA: 43.70000
LogP: 1.63350
Synthetic route
111-83-1

1-bromo-octane

111-42-2

2,2'-iminobis[ethanol]

15520-05-5

n-octyl dihydroxyethyl tertiary amine

Conditions
ConditionsYield
With potassium carbonate In acetonitrile for 12h; Inert atmosphere; Reflux;91%
In ethanol Heating; E. Wilson and M. Tishler, J. Am. Chem. Soc., 73, 3635 (1951);78%
With potassium carbonate; potassium iodide In acetonitrile for 12h; Inert atmosphere; Reflux;76.7%
111-85-3

1-Chlorooctane

111-42-2

2,2'-iminobis[ethanol]

15520-05-5

n-octyl dihydroxyethyl tertiary amine

Conditions
ConditionsYield
With sodium carbonate In acetonitrile for 9h; Heating;65%
In isopropyl alcohol at 140℃;
75-21-8

oxirane

111-86-4

n-Octylamine

15520-05-5

n-octyl dihydroxyethyl tertiary amine

Conditions
ConditionsYield
With water at 100 - 190℃;
111-42-2

2,2'-iminobis[ethanol]

CH3(CH2)5CH2CH2X

CH3(CH2)5CH2CH2X

15520-05-5

n-octyl dihydroxyethyl tertiary amine

Conditions
ConditionsYield
With potassium carbonate In chloroform at 20℃;
15520-05-5

n-octyl dihydroxyethyl tertiary amine

C28H34O9S2

N-octyl-8-benzyloxymethyl-4,7,10,13-tetraoxa-1-azacyclopentadecane

Conditions
ConditionsYield
With sodium t-butanolate In 1,4-dioxane; tert-butyl alcohol at 40℃; for 12h;56%
15520-05-5

n-octyl dihydroxyethyl tertiary amine

7460-82-4

diethylene glycol ditosylate

120547-32-2

10-octyl-1,4,7-trioxa-10-azacyclododecane

Conditions
ConditionsYield
With lithium; tert-butyl alcohol In 1,4-dioxane for 25h; Heating;38%
15520-05-5

n-octyl dihydroxyethyl tertiary amine

7705-08-0

iron(III) chloride

730959-69-0

Fe6Cl6((OC2H4)2N(CH2)7CH3)6

Conditions
ConditionsYield
With calcium hydride In tetrahydrofuran to a suspn. of CaH2 in anhydrous THF was added dihydroxyamine, stirred for 1 h at 20°C, a soln. of FeCl3 in anhydrous THF was added, the mixt. was stirred at 20°C for 72 h (N2); solvent was removed under vac., ppt. was dissolved in CH2Cl2, the residue was filtered off, evapd., recrystd. from CHCl3/n-pentane; elem. anal.;18%
54535-06-7

bis(o-phenylene)glycol ditosylate

15520-05-5

n-octyl dihydroxyethyl tertiary amine

N-octylbenzoaza-15-crown-5

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran for 45h; Heating;9%
15520-05-5

n-octyl dihydroxyethyl tertiary amine

52419-79-1

Bis-(2-chloro-ethyl)-octyl-amine

Conditions
ConditionsYield
With thionyl chloride In chloroform Heating;
15520-05-5

n-octyl dihydroxyethyl tertiary amine

Bis-(2-chloro-ethyl)-octyl-amine; hydrochloride

Conditions
ConditionsYield
With thionyl chloride In chloroform E. Wilson and M. Tishler, J. Am. Chem. Soc., 73, 3635 (1951);
With thionyl chloride
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