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CAS No.: | 15520-05-5 |
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Name: | 2,2'-(octylimino)bisethanol |
Article Data: | 10 |
Molecular Structure: | |
Formula: | C12H27 N O2 |
Molecular Weight: | 217.352 |
Synonyms: | Ethanol,2,2'-(octylimino)di- (8CI); 2,2'-(Octylimino)diethanol;Bis(2-hydroxyethyl)octylamine; Diethanoloctylamine; Hetoxamine OT 2;N,N-Bis(2-hydroxyethyl)octylamine; N-Octyldiethanolamine; Octyldiethanolamine |
Density: | 0.949g/cm3 |
Boiling Point: | 342.4°Cat760mmHg |
Flash Point: | 150.5°C |
Solubility: | 1.4g/L at 20℃ |
PSA: | 43.70000 |
LogP: | 1.63350 |
Conditions | Yield |
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With potassium carbonate In acetonitrile for 12h; Inert atmosphere; Reflux; | 91% |
In ethanol Heating; E. Wilson and M. Tishler, J. Am. Chem. Soc., 73, 3635 (1951); | 78% |
With potassium carbonate; potassium iodide In acetonitrile for 12h; Inert atmosphere; Reflux; | 76.7% |
Conditions | Yield |
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With sodium carbonate In acetonitrile for 9h; Heating; | 65% |
In isopropyl alcohol at 140℃; |
Conditions | Yield |
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With water at 100 - 190℃; |
2,2'-iminobis[ethanol]
n-octyl dihydroxyethyl tertiary amine
Conditions | Yield |
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With potassium carbonate In chloroform at 20℃; |
n-octyl dihydroxyethyl tertiary amine
Conditions | Yield |
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With sodium t-butanolate In 1,4-dioxane; tert-butyl alcohol at 40℃; for 12h; | 56% |
n-octyl dihydroxyethyl tertiary amine
diethylene glycol ditosylate
10-octyl-1,4,7-trioxa-10-azacyclododecane
Conditions | Yield |
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With lithium; tert-butyl alcohol In 1,4-dioxane for 25h; Heating; | 38% |
n-octyl dihydroxyethyl tertiary amine
iron(III) chloride
Fe6Cl6((OC2H4)2N(CH2)7CH3)6
Conditions | Yield |
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With calcium hydride In tetrahydrofuran to a suspn. of CaH2 in anhydrous THF was added dihydroxyamine, stirred for 1 h at 20°C, a soln. of FeCl3 in anhydrous THF was added, the mixt. was stirred at 20°C for 72 h (N2); solvent was removed under vac., ppt. was dissolved in CH2Cl2, the residue was filtered off, evapd., recrystd. from CHCl3/n-pentane; elem. anal.; | 18% |
bis(o-phenylene)glycol ditosylate
n-octyl dihydroxyethyl tertiary amine
Conditions | Yield |
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With sodium hydride In tetrahydrofuran for 45h; Heating; | 9% |
n-octyl dihydroxyethyl tertiary amine
Bis-(2-chloro-ethyl)-octyl-amine
Conditions | Yield |
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With thionyl chloride In chloroform Heating; |
n-octyl dihydroxyethyl tertiary amine
Conditions | Yield |
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With thionyl chloride In chloroform E. Wilson and M. Tishler, J. Am. Chem. Soc., 73, 3635 (1951); | |
With thionyl chloride |