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1944-63-4

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Basic Information
CAS No.: 1944-63-4
Name: 3-[(3AS,4S,7AS)-7A-METHYL-1,5-DIOXOOCTAHYDRO-1H-INDEN-4-YL]PROPIONIC ACID
Article Data: 8
Molecular Structure:
Molecular Structure of 1944-63-4 (3-[(3AS,4S,7AS)-7A-METHYL-1,5-DIOXOOCTAHYDRO-1H-INDEN-4-YL]PROPIONIC ACID)
Formula: C13H18 O4
Molecular Weight: 238.284
Synonyms: 1H-Indene-4-propanoicacid, octahydro-7a-methyl-1,5-dioxo-, [3aS-(3aa,4a,7ab)]-; 4-Indanpropionic acid, 3aa,4b,5,6,7,7a-hexahydro-7ab-methyl-1,5-dioxo- (6CI,7CI,8CI); 1,5-Dioxo-7ab-methyl-3aa-hexahydroindane-4a-propionic acid;7a-Methyl-1,5-dioxo-3aa,7ab-hexahydroindan-4a-yl propionic acid; 7ab-Methylhexahydroindane-1,5-dione-4a-(3-propionic acid)
PSA: 71.44000
LogP: 1.81570
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Synthetic route

C13H18O3

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

Conditions
ConditionsYield
With sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene In water; tert-butyl alcohol at 20℃; for 18h;40%
62026-31-7

[3-(2-methyl-[1,3]dioxolan-2-yl)-propyl]-magnesium chloride

74712-32-6, 88293-64-5

C18H26O5

A

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

B

71594-11-1

2,2-dimethyl-6-(2-methyl-[1,3]dioxolan-2-yl)-hexan-3-one

C

24894-29-9

(+)-3,3-ethylenedioxy-4,5-seco-19-norandrost-9-en-5,17-dione

Conditions
ConditionsYield
In tetrahydrofuran at -70℃; for 1h; Yield given;
...Expand
37134-59-1

(1R,3aS,4S,7aS)-4-(2-Carboxy-ethyl)-1-hydroxy-7a-methyl-5-oxo-octahydro-indene-1-carboxylic acid

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

Conditions
ConditionsYield
With sodium bismuthate In acetic acid
17553-86-5

(S)-Halos-Parish ketone

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

Conditions
ConditionsYield
Multi-step reaction with 8 steps
1.1: sodium tetrahydroborate / ethanol / 0 °C / Inert atmosphere
2.1: 1-methyl-1H-imidazole; iodine / tetrahydrofuran / 42 h / 20 °C / Inert atmosphere
3.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
3.2: 18 h / 20 °C / Inert atmosphere
4.1: palladium on activated charcoal; hydrogen
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
7.1: periodic acid / ethyl acetate / 20 °C
8.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
Multi-step reaction with 8 steps
1.1: sodium tetrahydroborate / ethanol / 0 °C / Inert atmosphere
2.1: 1-methyl-1H-imidazole; iodine / tetrahydrofuran / 42 h / 20 °C / Inert atmosphere
3.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
3.2: 18 h / 20 °C / Inert atmosphere
4.1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / methanol / 1 h / -35 °C
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
7.1: periodic acid / ethyl acetate / 20 °C
8.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
Multi-step reaction with 8 steps
1.1: sodium tetrahydroborate / ethanol / 0 °C / Inert atmosphere
2.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
3.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
3.2: 18 h / 20 °C / Inert atmosphere
4.1: palladium on activated charcoal; hydrogen
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
7.1: periodic acid / ethyl acetate / 20 °C
8.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
Multi-step reaction with 8 steps
1.1: sodium tetrahydroborate / ethanol / 0 °C / Inert atmosphere
2.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
3.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
3.2: 18 h / 20 °C / Inert atmosphere
4.1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / methanol / 1 h / -35 °C
5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
6.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
7.1: periodic acid / ethyl acetate / 20 °C
8.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme

C23H40O4Si

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / methanol / 1 h / -35 °C
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
4: periodic acid / ethyl acetate / 20 °C
5: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
Multi-step reaction with 5 steps
1: palladium on activated charcoal; hydrogen
2: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
3: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
4: periodic acid / ethyl acetate / 20 °C
5: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme

C23H42O4Si

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
2: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
3: periodic acid / ethyl acetate / 20 °C
4: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme

C17H28O4

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
2: periodic acid / ethyl acetate / 20 °C
3: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
16271-49-1

(1S,7aS)-1-hydroxy-7a-methyl-2,3,7,7a-tetrahydro-1H-inden-5(6H)-one

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

Conditions
ConditionsYield
Multi-step reaction with 7 steps
1.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
2.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
2.2: 18 h / 20 °C / Inert atmosphere
3.1: palladium on activated charcoal; hydrogen
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
6.1: periodic acid / ethyl acetate / 20 °C
7.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
Multi-step reaction with 7 steps
1.1: 2,6-dimethylpyridine / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere
2.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
2.2: 18 h / 20 °C / Inert atmosphere
3.1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / methanol / 1 h / -35 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
6.1: periodic acid / ethyl acetate / 20 °C
7.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
Multi-step reaction with 7 steps
1.1: 1-methyl-1H-imidazole; iodine / tetrahydrofuran / 42 h / 20 °C / Inert atmosphere
2.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
2.2: 18 h / 20 °C / Inert atmosphere
3.1: palladium on activated charcoal; hydrogen
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
6.1: periodic acid / ethyl acetate / 20 °C
7.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
Multi-step reaction with 7 steps
1.1: 1-methyl-1H-imidazole; iodine / tetrahydrofuran / 42 h / 20 °C / Inert atmosphere
2.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
2.2: 18 h / 20 °C / Inert atmosphere
3.1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / methanol / 1 h / -35 °C
4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
5.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
6.1: periodic acid / ethyl acetate / 20 °C
7.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme

C17H26O4

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: periodic acid / ethyl acetate / 20 °C
2: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
149789-99-1, 126541-53-5

(1S,7aS)-1-((tert-butyldimethylsilyl)oxy)-7a-methyl-1,2,3,6,7,7a-hexahydro-5H-inden-5-one

1944-63-4

3aα-H-4α-(3’-propionic acid)-7aβ-methylhexahydro-1,5-indanedione

Conditions
ConditionsYield
Multi-step reaction with 6 steps
1.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
1.2: 18 h / 20 °C / Inert atmosphere
2.1: nickel(II) chloride hexahydrate; sodium tetrahydroborate / methanol / 1 h / -35 °C
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
5.1: periodic acid / ethyl acetate / 20 °C
6.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
Multi-step reaction with 6 steps
1.1: dimethyl sulfoxide; sodium hydride / tetrahydrofuran; mineral oil / 2 h / 0 - 20 °C / Inert atmosphere
1.2: 18 h / 20 °C / Inert atmosphere
2.1: palladium on activated charcoal; hydrogen
3.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 18 h / 20 °C
4.1: 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione / dimethyl sulfoxide / 18 h / 20 °C
5.1: periodic acid / ethyl acetate / 20 °C
6.1: sodium chlorite; sodium dihydrogenphosphate dihydrate; 2-methyl-but-2-ene / water; tert-butyl alcohol / 18 h / 20 °C
View Scheme
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    FOB Price:  USD $ 0.0-0.0

    Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por

    Shanghai fine pharma co., Ltd. is a professional enterprise with chemical reagents and fine chemical products development, development and trade. The company has a sound research a

  • Shanghai Run-Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-21-31576854/57171705 / 57171706

    Address:second floor, building 3, No.999, jiangyue Road, minghang District, Shanghai, China

       Inquiry Now

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