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CAS No.: | 19829-72-2 |
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Name: | 2,3-Dihydroxyterephthalic acid |
Article Data: | 19 |
Molecular Structure: | |
Formula: | C8H6O6 |
Molecular Weight: | 198.132 |
Synonyms: | 1,4-Benzenedicarboxylic acid,2,3-dihydroxy;2,3-dihydroxy-terephthalic acid;2,3-dihydroxy-1,4-benzenedicarboxylic acid;EINECS 243-354-3;1,4-Benzenedicarboxylic acid, 2,3-dihydroxy-;2,3-Dihydroxy-terephthalsaeure; |
Density: | 1.779g/cm3 |
Melting Point: | 309-310℃ (ethanol ethyl ether ) |
Boiling Point: | 456.5°C at 760 mmHg |
Flash Point: | 244°C |
PSA: | 115.06000 |
LogP: | 0.49420 |
Conditions | Yield |
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Stage #1: carbon dioxide; benzene-1,2-diol With potassium carbonate at 230 - 250℃; under 19652.1 - 60507.9 Torr; for 19.25h; Stage #2: With hydrogenchloride In water for 5h; | 95% |
With sodium hydroxide 1.) MeOH, r.t., 15 min, 2.) 1100 psi, 195-200 deg C, 90 h; | 56% |
Stage #1: benzene-1,2-diol With sodium hydroxide Stage #2: carbon dioxide at 200℃; under 60800 Torr; for 48h; | 54% |
Conditions | Yield |
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With 1,2,4-Trichlorobenzene at 225℃; for 14h; Autoclave; | 73% |
3,6-dicyanocatechol
2,3-dihydroxyterephthalic acid
Conditions | Yield |
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With sodium hydroxide |
2,3-dimethoxyterephthalic acid
2,3-dihydroxyterephthalic acid
Conditions | Yield |
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With hydrogen bromide |
Conditions | Yield |
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at 225℃; |
Conditions | Yield |
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at 200℃; im Rohr; |
benzene-1,2-diol
glycerol
A
2,3-Dihydroxybenzoic acid
B
2,3-dihydroxyterephthalic acid
Conditions | Yield |
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at 180℃; |
carbon dioxide
2,3-dihydroxyterephthalic acid
Conditions | Yield |
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unter hohem Druck und man erhitzt das gebildete Salz bei Gegenwart von CO2 im Autoklaven auf 210grad; |
benzene-1,2-diol
2,3-dihydroxyterephthalic acid
Conditions | Yield |
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at 200℃; im Einschlussrohr; |
2,3-dihydroxyterephthalic acid
Conditions | Yield |
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With glycerol at 210℃; |