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Basic Information
| CAS No.: | 204-02-4 |
|---|---|
| Name: | perimidine |
| Article Data: | 34 |
| Molecular Structure: | |
|
|
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| Formula: | C11H8 N2 |
| Molecular Weight: | 168.198 |
| Synonyms: | Perimidine(6CI,7CI,8CI); 1,3-Diaza-1H-benzonaphthene; 1H-Benzo[de]quinazoline |
| Density: | 1.26g/cm3 |
| Melting Point: | 223°C |
| Boiling Point: | 371.1°Cat760mmHg |
| Flash Point: | 178.2°C |
| PSA: | 28.68000 |
| LogP: | 2.71610 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: orthoformic acid triethyl ester at 20℃; for 0.25h; Stage #2: naphthalene-1,8-diamine at 20℃; for 3h; | 100% |
Conditions
| Conditions | Yield |
|---|---|
| In formic acid; hydrogen bromide for 1.5h; Heating; | 97% |
Conditions
| Conditions | Yield |
|---|---|
| In ethanol | 96% |
| In ethanol for 0.666667h; Heating; | 95% |
| With hydrogen bromide In acetone Reflux; | 95% |
- 69098-80-2
2,3-dihydroperimidine
- 204-02-4
1-H-perimidine
Conditions
| Conditions | Yield |
|---|---|
| With sodium disulfite In ethanol; water for 2h; Heating; | 95% |
Conditions
| Conditions | Yield |
|---|---|
| With carbon dioxide In water at 150℃; under 37503.8 Torr; for 5h; | 93.1% |
| With 1,1,1,3,3,3-hexamethyl-disilazane at 120℃; for 12h; Green chemistry; | 50% |
| With zinc(II) acetate dihydrate In neat (no solvent) at 120℃; under 7600.51 Torr; for 18h; Autoclave; Inert atmosphere; Green chemistry; | 41% |
- 121766-89-0
benzylpenicilloic acid α-phenylethylamide
- 479-27-6
naphthalene-1,8-diamine
A
- 204-02-4
1-H-perimidine
B
- 52-67-5
3,3-dimethyl-D-cysteine
C
- 102016-26-2
phenaceturic acid α-phenethylamide
Conditions
| Conditions | Yield |
|---|---|
| In water; acetic acid for 2h; Heating; | A 85% B 69% C 74% |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| With [(N,N′-bis(diisopropylphosphino)-2,6-diaminopyridine)Mn(CO)3][Br]; potassium tert-butylate In toluene at 120℃; for 24h; Inert atmosphere; Glovebox; Schlenk technique; | 69% |
Conditions
| Conditions | Yield |
|---|---|
| With 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine In toluene at 100℃; under 22502.3 Torr; for 48h; Autoclave; | 66% |
Conditions
| Conditions | Yield |
|---|---|
| In toluene at 100℃; for 48h; | 44% |
Conditions
| Conditions | Yield |
|---|---|
| With 1,1,1,3,3,3-hexamethyl-disilazane at 120℃; for 12h; Green chemistry; | 38% |
- Total:15 Page 1 of 1 1
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