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23582-06-1

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Basic Information
CAS No.: 23582-06-1
Name: [2-(diphenylarsino)ethyl]diphenylphosphine
Molecular Structure:
Molecular Structure of 23582-06-1 ([2-(diphenylarsino)ethyl]diphenylphosphine)
Formula: C26H24 As P
Molecular Weight: 442.372
Synonyms: 1-(Diphenylarsino)-2-(diphenylphosphino)ethane;1-(Diphenylphosphino)-2-(diphenylarsino)ethane; 2-(Diphenylphosphinoethyl)diphenylarsine;Arphos; [2-(Diphenylarsino)ethyl]diphenylphosphine
Density: g/cm3
Boiling Point: 518.1°Cat760mmHg
Flash Point: 283.9°C
PSA: 13.59000
LogP: 4.42850
Related products
Synthetic route
12146-37-1, 124717-04-0

(bicyclo[2.2.1]hepta-2,5-diene)tetracarbonylmolybdenum(0)

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

A

53557-42-9

(1-diphenylphosphino-2-diphenylarsinoethane)molybdenum tetracarbonyl

B

121-46-0

bicyclo[2.2.1]hepta-2,5-diene

Conditions
ConditionsYield
In tetrahydrofuran reaction in a calorimeter under argon;A 100%
B n/a
...Expand
1174037-38-7

[Pd(3,4-Me2C6H2C(Me)=NN(H)(3'-(CF3)C4H2N2))Cl]

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

sodium perchlorate

2923-28-6

silver trifluoromethanesulfonate

1174037-43-4

[Pd(3,4-Me2C6H2C(Me)=NN(H)(3'-(CF3)C4H2N2))(PPh2(CH2)2AsPh2)]ClO4

Conditions
ConditionsYield
In acetone byproducts: AgCl; Ag salt was added to soln. of Pd complex in acetone; stirred for 4 h; filtered through Celite; P-As ligand was added to filtrate; stirred for 2 h; NaClO4 was added; stirred for 1 h; H2O added; filtered; dried (vac.); elem. anal.;99%
...Expand

ammonium hexafluorophosphate

chloro(η5-cyclopentadienyl)(1,10-phenanthroline)ruthenium(II)

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

109011-10-1

bis(η5-cyclopentadienyl)bis(1,10-phenanthroline)(μ-1-(diphenylphosphino)-2-(diphenylarsino)ethane)diruthenium(II) hexafluorophosphate

Conditions
ConditionsYield
In ethanol a suspn. of Ru-complex in EtOH was treated with an ethanol soln. of dppae under inert atmosphere, mixt. was heated under reflux for 20 min, filtered, cooled to room temp., a soln. of NH4PF6 in EtOH was added; ppt. was isolated by filtration, washed with Et2O; elem. anal.;98%
...Expand
84651-76-3

(η-cyclopentadienyl)(η-cyclopentadiene)nickel tetrafluoroborate

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

A

85412-97-1

cyclopentadienylnickel(diphenylphosphino(diphenylarsino)ethylidene)

B

542-92-7

cyclopenta-1,3-diene

Conditions
ConditionsYield
In chloroform under Ar, Ni complex and ligand stirred in CHCl3 for 5 min; filtered, filtrate dropped in ether, filtered, dried in vac., elem. anal.;A 93%
B n/a
...Expand

ammonium hexafluorophosphate

174865-79-3

[Pd(5-(COH)C6H3C(H)N(cyclohexyl)-C2,N)(μ-Cl)]2

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

523977-74-4

[Pd(4-(COH)C6H3C(H)=NCy-C2,N)(1-diphenylphosphino-2-diphenylarsinoethane-P,As)][PF6]

Conditions
ConditionsYield
In acetone ligand (2 equiv.) added to soln. of Pd complex in acetone; stirred at room temp. for 2 h; NH4PF6 (1 equiv.) added; stirred for 1 h; water added dropwise; stirred for 2 h; filtered; ppt. washed with water; dried in vac. over anhyd. CaCl2; recrystd. from CH2Cl2-n-hexane; elem. anal.;88%
...Expand

[Pd(CH2CMe2PtBu2)(μ-Cl)]2

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

Pd(2+)*Cl(1-)*((CH3)3C)2PC4H8(1-)*(C6H5)2PCH2CH2As(C6H5)2=(PdCl(((CH3)3C)2PC(CH3)2CH2)((C6H5)2PCH2CH2As(C6H5)2))

Conditions
ConditionsYield
In benzene to stirred soln. (Pt2Cl2(Bu2tPCMe2CH2)2) in benzene added ape and react. mixt. stirred at 40°C for 5 h under N2 atm.; soln. concd., hexane added, solid filtered, washed with ether and vac. dried; elem. anal.;86%
50978-00-2

chloro(methyl)(1,5-cyclooctadiene)platinum(II)

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

PtCH3Cl(C6H5)2AsCH2CH2P(C6H5)2

Conditions
ConditionsYield
In dichloromethane ligand was added to soln. of the Pt complex in CH2Cl2, mixt. stirred at room temp. for 1 h; concd., filtered, washed with hexane and ether, dried under reduced pressure; elem. anal.;86%

ammonium hexafluorophosphate

174865-79-3

[Pd(5-(COH)C6H3C(H)N(cyclohexyl)-C2,N)(μ-Cl)]2

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

521070-28-0

[Pd(5-(COH)C6H3C(H)=NCy-C2,N)(1-diphenylphosphino-2-diphenylarsinoethane-P,As)][PF6]

Conditions
ConditionsYield
With silver trifluorosulfonate In acetone byproducts: AgCl; AgOSO2CF3 (1 equiv.) added to soln. of Pd complex in acetone; stirred for 1 h; filtered through Celite; ligand (2 equiv.) and NH4PF6 (3 equiv.) added to soln.; stirred for 12 h; filtered; ppt. recrystd. from CHCl3-n-hexane; elem. anal.;86%
...Expand
13755-29-8

sodium tetrafluoroborate

308108-82-9

[Pt(6-neo-pentyl-2,2'-bipyridine(1-)κC,κ2N,N')Cl]

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

507271-10-5

[Pt(C10H7N2CH2C(CH3)2CH2)(C6H5)2PCH2CH2As(C6H5)2](1+)*BF4(1-)=[[PtC10H7N2CH2C(CH3)2CH2](C6H5)2PCH2CH2As(C6H5)2](BF4)

Conditions
ConditionsYield
In acetone NaBF4 was added to Me2CO soln. of 1 equiv. of Pt- and 1 equiv. of P-compd., resp., mixt. was stirred in for 4 h; solvent was evapd. to dryness, residue was recrystd. from CH2Cl2/Et2O, elem. anal.;84%
...Expand

Rh(1,5-cyclooctadiene)(η3-2-Me-allyl)

23582-06-1

1-diphenylarsino-2-diphenylphosphinoethane

81178-02-1

[η3-(2-Me-C3H4)Rh(arphos)]

Conditions
ConditionsYield
In hexane; dichloromethane a soln. of ligand in CH2Cl2 was added a soln. of complex in hexane and stirred for 0.5 h, N2 atm.; evapn. in vac., repptn. from CH2Cl2 with hexane at -30°C; elem. anal.;83%
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