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Basic Information
| CAS No.: | 2415-93-2 |
|---|---|
| Name: | 1-(3-BROMOPHENYL)-2-METHYLPROPAN-1-ONE |
| Article Data: | 9 |
| Molecular Structure: | |
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| Formula: | C10H11 Br O |
| Molecular Weight: | 227.101 |
| Synonyms: | Propiophenone,3'-bromo-2-methyl- (7CI,8CI); 1-Bromo-3-isobutyrylbenzene |
| Density: | 1.331g/cm3 |
| Boiling Point: | 279.9°Cat760mmHg |
| Flash Point: | 63.4°C |
| PSA: | 17.07000 |
| LogP: | 3.28780 |
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Synthetic route
- 67-56-1
methanol
- 19829-31-3
1-(3-bromophenyl)-1-propanone
- 2415-93-2
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions
| Conditions | Yield |
|---|---|
| With C34H27IrN2P(1+)*C32H12BF24(1-); caesium carbonate at 65℃; for 24h; Inert atmosphere; | 93% |
| With C21H17ClN5ORu(1+)*Cl(1-); potassium tert-butylate at 85℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 87% |
| With C34H27MnNO3P2(1+)*Br(1-); caesium carbonate at 85℃; for 24h; Schlenk technique; Inert atmosphere; | 79% |
Conditions
| Conditions | Yield |
|---|---|
| With C21H17ClN5ORu(1+)*Cl(1-); potassium tert-butylate at 100℃; for 24h; Inert atmosphere; Schlenk technique; Glovebox; Sealed tube; | 87% |
- 2403-57-8
1-(2-methylprop-1-en-1-yl)pyrrolidine
- 35306-75-3
3-bromobenzoic acid isopropylamide
- 2415-93-2
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 3-bromobenzoic acid isopropylamide With 2-fluoropyridine; trifluoromethylsulfonic anhydride In dichloromethane at 0℃; for 0.333333h; Stork Enamine Alkylation; Inert atmosphere; Schlenk technique; Stage #2: 1-(2-methylprop-1-en-1-yl)pyrrolidine In dichloromethane at 0 - 20℃; for 3h; Stork Enamine Alkylation; Inert atmosphere; Schlenk technique; Stage #3: With hydrogenchloride In dichloromethane; water at 20℃; Stork Enamine Alkylation; Inert atmosphere; Schlenk technique; | 81% |
- 1711-09-7
3-bromobenzoyl chloride
- 1068-55-9
isopropylmagnesium chloride
- 2415-93-2
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions
| Conditions | Yield |
|---|---|
| With Bis<2-(N,N-dimethylamino)aethyl>aether In tetrahydrofuran Grignard reaction; cooling; | 75% |
- 7194-78-7
(3-bromophenyl)oxoacetic acid
- 78-84-2
isobutyraldehyde
- 2415-93-2
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions
| Conditions | Yield |
|---|---|
| With dipotassium peroxodisulfate; iron(III)-acetylacetonate; di-tert-butyl peroxide In ethyl acetate at 120℃; for 2h; Sealed tube; | 65% |
| With dipotassium peroxodisulfate; iron(III)-acetylacetonate; di-tert-butyl peroxide In ethyl acetate at 120℃; for 12h; | 65% |
- 19829-31-3
1-(3-bromophenyl)-1-propanone
- 74-88-4
methyl iodide
- 2415-93-2
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions
| Conditions | Yield |
|---|---|
| (i) NaNH2, toluene, (ii) /BRN= 969135/; Multistep reaction; |
- 2415-93-2
1-(3-bromophenyl)-2-methylpropane-1-one
Conditions
| Conditions | Yield |
|---|---|
| With aluminum oxide; pyridinium chlorochromate In dichloromethane at 20℃; for 1h; | 2.1 g |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: m-trifluoromethylphenyl iodide With TurboGrignard In tetrahydrofuran at -20℃; for 0.5h; Inert atmosphere; Stage #2: 1-(3-bromophenyl)-2-methylpropane-1-one With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate In tetrahydrofuran at 25℃; for 0.0833333h; Kumada coupling reaction; Inert atmosphere; | 87% |
Conditions
| Conditions | Yield |
|---|---|
| With sodium t-butanolate In tetrahydrofuran at 20℃; for 1h; Inert atmosphere; | 86% |
Raw Materials
- Total:21 Page 1 of 1 1
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1-(3-BROMOPHENYL)-2-METHYLPROPAN-1-ONE
