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Basic Information
| CAS No.: | 2571-06-4 |
|---|---|
| Name: | Gallium acetate |
| Molecular Structure: | |
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| Formula: | C6H9GaO6 |
| Molecular Weight: | 246.857 |
| Synonyms: | acetic acid,gallium acetate;3,4-Dihydroxy-trans-zimtsaeure-propylester;3,4-dihydroxy-trans-cinnamic acid propyl ester;Essigsaeure,Galliumacetat;galium acetate;galinosoate C;n-propyl caffeate; |
| Density: | g/cm3 |
| Boiling Point: | 117.1°Cat760mmHg |
| Flash Point: | 40°C |
| PSA: | 78.90000 |
| LogP: | -0.33940 |
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Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| for 2h; Reflux; | 97.6% |
Conditions
| Conditions | Yield |
|---|---|
| With acetic anhydride In octane at 80℃; for 1.33333h; | 81% |
...Expand
- 2571-06-4
gallium(III) triacetate
Conditions
| Conditions | Yield |
|---|---|
| With triethylamine In methanol; chloroform soln. ligand in MeOH was added to refluxing MeOH, Ga(OAc)3 was added followed by a few drops Et3N, heated at reflux for 1 h; solvent was removed, chromy. on alumina (CH2Cl2-hexane 1:1) - mixt. of isomers; | 71% |
| With triethylamine In chloroform; N,N-dimethyl-formamide soln. ligand in MeOH was added to DMF at 150°C, Ga(OAc)3 was added followed by a few drops Et3N, heated at 150°C for 1 h; solvent was removed, chromy. on alumina (CH2Cl2-hexane 1:1) - mixt. of isomers; |
- 2571-06-4
gallium(III) triacetate
Conditions
| Conditions | Yield |
|---|---|
| In neat (no solvent) thermal decompn. of Ga-acetate; heating the amorphous intermediate at 480 to 600 °C; | |
| In neat (no solvent) thermal decompn. of Ga-acetate; heating the amorphous intermediate at 480 to 600 °C; |
Conditions
| Conditions | Yield |
|---|---|
| In water gallium acetatet and hexamolybdochromic acid in water at room temp.; concn. in a dessicator over KOH for weeks, crystals filtered off, washedwith water, ethanol, dried, recrystn. from hot water; elem. anal.; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In water in an aq. soln. at room temp.; concn. over KOH, crystn. for weeks, filtration, washing with H2O and EtOH, drying, recrystn. from hot H2O; elem. anal.; |
...Expand
- 2571-06-4
gallium(III) triacetate
Conditions
| Conditions | Yield |
|---|---|
| In water mixing, pptn. on standing (3 weeks); filtration, washing (cold water, ethanol), drying (room temp.); |
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Gallium acetate
