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27650-86-8

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Basic Information
CAS No.: 27650-86-8
Name: Naphthalene, 1-(3-bromopropyl)-
Article Data: 12
Molecular Structure:
Molecular Structure of 27650-86-8 (Naphthalene, 1-(3-bromopropyl)-)
Formula: C13H13Br
Molecular Weight: 249.15
Synonyms: 1-(3-Brom-propyl)-naphthalin;Naphthalene,1-(3-bromopropyl);1-(3-bromo-propyl)-naphthalene;3-(1-naphthalenyl)-propylbromide;
PSA: 0.00000
LogP: 4.16730
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27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
With carbon tetrabromide; TOP Ambient temperature;95%
With phosphorus tribromide In dichloromethane at 0 - 20℃;81%
With sulfuric acid; hydrogen bromide; acetic acid
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1-(3-bromo-n-propyl)-1,2,3,4-tetrahydronaphthalene

27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
With 2,3-dicyano-5,6-dichloro-p-benzoquinone In toluene for 4h; Heating;70%
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sodium diethylmalonate

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27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
Multistep reaction;
90-12-0

1-Methylnaphthalene

Mn(acac)3

Mn(acac)3

27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: BuLi; N,N,N',N'-tetramethylethylendiamine (TMEDA) / diethyl ether
2: TsOH (p-toluenesulphonic acid) / methanol
3: Ph3PBr2
View Scheme
400616-44-6

2-(3-naphthalen-1-yl-propoxy)-tetrahydro-pyran

27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: TsOH (p-toluenesulphonic acid) / methanol
2: Ph3PBr2
View Scheme
3243-42-3

1-Naphthalenepropanoic acid

27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: 97 percent / LiAlH4 / tetrahydrofuran
2: 95 percent / CBr4, tri-n-octylphosphine / Ambient temperature
View Scheme
13686-49-2

1-(2-bromo)ethylnaphthalene

27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1: 72 percent / ethanol; H2O / 21 h / Heating
2: 94 percent / 40percent aq. H2SO4 / 20 h / Heating
3: 97 percent / LiAlH4 / tetrahydrofuran
4: 95 percent / CBr4, tri-n-octylphosphine / Ambient temperature
View Scheme
70067-70-8

3-(naphthalen-1-yl)propanenitrile

27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 94 percent / 40percent aq. H2SO4 / 20 h / Heating
2: 97 percent / LiAlH4 / tetrahydrofuran
3: 95 percent / CBr4, tri-n-octylphosphine / Ambient temperature
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36060-99-8

3-(naphthalen-1-yl)propionic acid methyl ester

27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: LiAlH4; diethyl ether
2: red phosphorus; H2SO4; aqueous HBr
View Scheme
703-55-9

1-naphthylmagnesiumbromide

27650-86-8

1-(3-bromopropyl)naphthalene

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: diethyl ether; benzene
2: H2SO4; acetic acid; aqueous HBr
View Scheme
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