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Basic Information
| CAS No.: | 30508-27-1 |
|---|---|
| Name: | licoricidin |
| Molecular Structure: | |
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| Formula: | C26H32 O5 |
| Molecular Weight: | 424.537 |
| Synonyms: | 1,3-Benzenediol,4-[(3R)-3,4-dihydro-7-hydroxy-5-methoxy-6-(3-methyl-2-butenyl)-2H-1-benzopyran-3-yl]-2-(3-methyl-2-butenyl)-(9CI); 1,3-Benzenediol,4-[3,4-dihydro-7-hydroxy-5-methoxy-6-(3-methyl-2-butenyl)-2H-1-benzopyran-3-yl]-2-(3-methyl-2-butenyl)-,(R)-; 2',4',5-Isoflavantriol, 7-methoxy-3',6-bis(3-methyl-2-butenyl)- (8CI);(+)-Licoricidin; 7-O-Demethyllicorisoflavan A; Licoricidin; Licorisoflavan B |
| Density: | 1.171g/cm3 |
| Melting Point: | 161.0-162.5℃ |
| Boiling Point: | 610.8°Cat760mmHg |
| Flash Point: | 323.2°C |
| PSA: | 79.15000 |
| LogP: | 5.54810 |
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Synthetic route
- 30508-27-1
(+)-(R)-licoricidin
- 77-78-1
dimethyl sulfate
Conditions
| Conditions | Yield |
|---|---|
| With potassium carbonate In acetone |
Conditions
| Conditions | Yield |
|---|---|
| In pyridine |
- 30508-27-1
(+)-(R)-licoricidin
Conditions
| Conditions | Yield |
|---|---|
| With hydrogenchloride In methanol |
- 30508-27-1
(+)-(R)-licoricidin
- 1346768-14-6
4',7-dihydroxy-5-methoxy-6,3'-diprenylisoflavanquinone
Conditions
| Conditions | Yield |
|---|---|
| With sodium hydroxide In ethanol for 2h; |
- 30508-27-1
(+)-(R)-licoricidin
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: pyridine / 16 h 2: palladium dichloride / ethanol; water / 48 h / 20 °C View Scheme |
Conditions
| Conditions | Yield |
|---|---|
| With 2,3-dicyano-5,6-dichloro-p-benzoquinone In benzene for 0.0833333h; Reflux; | A 1 mg B 9.9 mg |
Conditions
| Conditions | Yield |
|---|---|
| With palladium dichloride In ethanol at 20℃; for 4h; | A 5.2 mg B 3.2 mg C 7.6 mg |
...Expand
- 30508-27-1
(+)-(R)-licoricidin
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 3 steps 1: pyridine / 16 h 2: palladium dichloride / ethanol; water / 48 h / 20 °C 3: sodium hydroxide; water / 0.5 h View Scheme |
- 108-24-7
acetic anhydride
- 30508-27-1
(+)-(R)-licoricidin
A
- 1542237-27-3
7,2'-diacetyllicoricidin
B
- 1542237-28-4
7,4'-diacetyllicoricidin
C
- 1542237-29-5
2',4'-diacetyllicoricidin
Conditions
| Conditions | Yield |
|---|---|
| With pyridine for 16h; | A 24.2 mg B 6.7 mg C 54.6 mg |
...Expand
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licoricidin
