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CAS No.: | 3069-25-8 |
---|---|
Name: | N-Methylaminopropyltrimethoxysilane |
Article Data: | 7 |
Molecular Structure: | |
Formula: | C7H19NO3Si |
Molecular Weight: | 193.318 |
Synonyms: | Propylamine,N-methyl-3-(trimethoxysilyl)- (7CI,8CI);(Methylaminopropyl)trimethoxysilane;(N-Methyl-3-aminopropyl)trimethoxysilane;(N-Methylaminopropyl)trimethoxysilane;(Trimethoxysilylpropyl)methylamine;3-(N-Methylaminopropyl)trimethoxysilane;Dynasylan 1110;N-Methyl-3-(trimethoxysilyl)-1-propanamine;N-Methyl-3-(trimethoxysilyl)propylamine;N-Methyl-g-aminopropyltrimethoxysilane;N-[3-(Trimethoxysilyl)propyl)methanamine;Silane 1110;Trimethoxy(3-(methylamino)propyl)silane;X 12-636;XZ 2024;[3-(Methylamino)propyl]trimethoxysilane;Trimethoxy[3-(methylamino)propyl]silane; |
EINECS: | 221-334-5 |
Density: | 0.93 g/cm3 |
Boiling Point: | 181.9 °C at 760 mmHg |
Flash Point: | 63.8 °C |
Solubility: | Hydrolyzes in water. |
Hazard Symbols: | Xi |
Risk Codes: | 36/37/38 |
Safety: | 26-36 |
PSA: | 39.72000 |
LogP: | 0.86490 |
N-methyl-N-allylamine
trimethoxysilane
A
N-methyl-3-trimethoxysilylpropylamine
Conditions | Yield |
---|---|
With platinum(0)-1,3-divinyl-1,1,3,3-tetramethyldisiloxane complex at 80℃; for 20h; Schlenk technique; Inert atmosphere; Overall yield = 93.2 %Spectr.; regioselective reaction; |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; | 100% |
2-Isocyanatoethyl methacrylate
N-methyl-3-trimethoxysilylpropylamine
3,3-dimethoxy-7-methyl-8-oxo-2-oxa-7,9-diaza-3-silaundecan-11-yl methacrylate
Conditions | Yield |
---|---|
at 60℃; | 100% |
Conditions | Yield |
---|---|
In tetrahydrofuran at 20℃; for 0.5h; | 99% |
Conditions | Yield |
---|---|
With potassium carbonate In toluene for 16h; Reflux; Inert atmosphere; | 96% |
N-methyl-3-trimethoxysilylpropylamine
hexafluoroglutaric anhydride
silver(l) oxide
(H3CO)3Si(CH2)3N(CH3)C(O)(CF2)3COO(1-)*Ag(1+)=Ag[(H3CO)3Si(CH2)3N(CH3)C(O)(CF2)3COO]
Conditions | Yield |
---|---|
In further solvent(s) under Ar, Schlenk setup, glutaric anhydride (1.4 mmol) in MTBE added to soln. of silicon compd. (1.4 mmol), stirred for 10 min, added to Ag2O (1.4 mmol) suspd. in MTBE, stirred for 18 h at room temp. in darkness; evapd. (vac.), elem. anal.; | 93% |
Conditions | Yield |
---|---|
Stage #1: N-methyl-3-trimethoxysilylpropylamine With trimethylamine In dichloromethane at 0℃; for 0.166667h; Inert atmosphere; Stage #2: acetyl chloride In dichloromethane for 4.5h; | 85% |
N-methyl-3-trimethoxysilylpropylamine
bis(trifluoromethanesulfonyl)amide
Conditions | Yield |
---|---|
In water; dimethyl sulfoxide at 25 - 100℃; for 19h; | 84% |
Conditions | Yield |
---|---|
at 130℃; for 3h; Inert atmosphere; Industrial scale; | 80% |
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IUPAC Name: N-Methyl-3-trimethoxysilylpropan-1-amine
Systematic of 1-Propanamine,N-methyl-3-(trimethoxysilyl)- (CAS NO.3069-25-8): EINECS 221-334-5 ; N-Methylaminopropyltrimethoxysilane
CAS NO: 3069-25-8
Molecular Formula of 1-Propanamine,N-methyl-3-(trimethoxysilyl)- (CAS NO.3069-25-8): C7H19NO3Si
Molecular Weight: 193.3162
Molecular Structure:
Polar Surface Area: 30.93 Å2
Index of Refraction: 1.415
Molar Refractivity: 52.02 cm3
Molar Volume: 207.7 cm3
Surface Tension: 23.3 dyne/cm
Density of 1-Propanamine,N-methyl-3-(trimethoxysilyl)- (CAS NO.3069-25-8): 0.93 g/cm3
Flash Point: 63.8 °C
Enthalpy of Vaporization: 41.81 kJ/mol
Boiling Point: 181.9 °C at 760 mmHg
Vapour Pressure: 0.834 mmHg at 25°C
Hazard Codes: Xi
Risk Statements: 36/37/38
R36/37/38: Irritating to eyes, respiratory system and skin.
Safety Statements: 26-36
S26: In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
S36: Wear suitable protective clothing.
WGK Germany: 3
TSCA: Yes