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Basic Information
| CAS No.: | 34888-05-6 |
|---|---|
| Name: | (trichloromethoxy)benzene |
| Article Data: | 9 |
| Molecular Structure: | |
|
|
|
| Formula: | C7H5 Cl3 O |
| Molecular Weight: | 211.475 |
| Synonyms: | Anisole, a,a,a-trichloro- (6CI); Phenyl trichloromethyl ether; Trichloromethyl phenylether; a,a,a-Trichloroanisole |
| Density: | 1.432g/cm3 |
| Boiling Point: | 237°Cat760mmHg |
| Flash Point: | 90.6°C |
| PSA: | 9.23000 |
| LogP: | 3.39310 |
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Synthetic route
- 456-55-3
1-trifluoromethoxybenzene
A
- 34888-05-6
(trichloromethoxy)benzene
B
- 1544-69-0
α,α,α-dichlorofluoromethoxybenzene
Conditions
| Conditions | Yield |
|---|---|
| With aluminium trichloride In dichloromethane at 0 - 10℃; for 0.5h; | A 98.2% B 1.8% |
- 456-55-3
1-trifluoromethoxybenzene
- 75-36-5
acetyl chloride
A
- 34888-05-6
(trichloromethoxy)benzene
B
- 85013-98-5
1-[4-(trifluoromethoxy)phenyl]ethan-1-one
Conditions
| Conditions | Yield |
|---|---|
| With aluminium trichloride In tetrachloromethane for 2h; Product distribution; Further Variations:; Solvents; | A 80% B 20% |
...Expand
- 98273-25-7
dichloro-phenoxy-methanesulfenyl chloride
- 34888-05-6
(trichloromethoxy)benzene
Conditions
| Conditions | Yield |
|---|---|
| With chlorine |
- 56-23-5
tetrachloromethane
- 108-95-2
phenol
A
- 34888-05-6
(trichloromethoxy)benzene
B
- 17696-62-7
Phenyl 4-hydroxybenzoate
C
- 118-55-8
phenyl Salicylate
D
- 1441-87-8
salicyloyl chloride
Conditions
| Conditions | Yield |
|---|---|
| for 5h; Irradiation; Yield given. Yields of byproduct given; |
...Expand
- 1005-56-7
phenylcarbonochloridothioate
- 34888-05-6
(trichloromethoxy)benzene
Conditions
| Conditions | Yield |
|---|---|
| Multi-step reaction with 2 steps 1: chlorine 2: chlorine View Scheme |
- 456-55-3
1-trifluoromethoxybenzene
- 34888-05-6
(trichloromethoxy)benzene
Conditions
| Conditions | Yield |
|---|---|
| With aluminum (III) chloride In benzene-d6; chlorobenzene at 80℃; for 42h; |
- 100-66-3
methoxybenzene
- 34888-05-6
(trichloromethoxy)benzene
Conditions
| Conditions | Yield |
|---|---|
| With chlorine; 4-chlorobenzotrifluoride at 90 - 100℃; UV-irradiation; | |
| With 2,2'-azobis(isobutyronitrile); chlorine at 139 - 140℃; for 12h; Temperature; |
- 34888-05-6
(trichloromethoxy)benzene
- 456-55-3
1-trifluoromethoxybenzene
Conditions
| Conditions | Yield |
|---|---|
| With hydrogen fluoride at 95℃; under 21002.1 Torr; Temperature; Pressure; Autoclave; | 95.46% |
| 90% | |
| With antimonypentachloride; antimony(III) fluoride |
- 34888-05-6
(trichloromethoxy)benzene
- 770-11-6
difluorochloromethoxybenzene
Conditions
| Conditions | Yield |
|---|---|
| With perfluorooctyl sulfofluorure; hydrogen fluoride at 5 - 110℃; under 18751.9 - 21002.1 Torr; for 4h; Autoclave; | 74.9% |
| With antimony(III) fluoride | |
| With (HF)10-pyridine at 20℃; for 6h; | 97 % Spectr. |
| With hydrogen fluoride at 50℃; under 7500.75 Torr; for 1h; Autoclave; | |
| With hydrogen fluoride at 50℃; under 7500.75 Torr; Inert atmosphere; Autoclave; |
- Total:13 Page 1 of 1 1
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(trichloromethoxy)benzene
