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CAS No.: | 3490-06-0 | ||||||||||||||
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Name: | N-methylhomoveratrylamine | ||||||||||||||
Article Data: | 29 | ||||||||||||||
Molecular Structure: | |||||||||||||||
Formula: | C11H17 N O2 | ||||||||||||||
Molecular Weight: | 195.261 | ||||||||||||||
Synonyms: | Phenethylamine,3,4-dimethoxy-N-methyl- (6CI,7CI,8CI);2-(3,4-Dimethoxyphenyl)-N-methylethanamine; 2-(3,4-Dimethoxyphenyl)-N-methylethylamine;3,4-Dimethoxy-N-methylbenzeneethanamine; 3,4-Dimethoxy-N-methylphenethylamine;3,4-Dimethoxy-N-methylphenylethylamine; 3,4-Dimethoxy-b-phenethylmethylamine;Methyl[2-(3,4-dimethoxyphenyl)ethyl]amine; N-(3,4-Dimethoxyphenethyl)-N-methylamine;N-Methyl-2-(3,4-dimethoxyphenyl)ethylamine; N-Methyl-3,4-dimethoxy-b-phenethylamine;N-Methyl-3,4-dimethoxy-b-phenylethylamine; N-Methyl-3,4-dimethoxybenzeneethanamine;N-Methyl-3,4-dimethoxyphenethylamine; N-Methylhomoveratrylamine; N-[2-(3,4-Dimethoxyphenyl)ethyl]-N-methylamine;NSC 187772; [2-(3,4-Dimethoxyphenyl)ethyl]methylamine | ||||||||||||||
EINECS: | 222-483-9 | ||||||||||||||
Density: | 1.059 | ||||||||||||||
Boiling Point: | 294.4°Cat760mmHg | ||||||||||||||
Flash Point: | >110 ºC | ||||||||||||||
Hazard Symbols: | |||||||||||||||
Risk Codes: | R36/37/38 | ||||||||||||||
Safety: |
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PSA: | 30.49000 | ||||||||||||||
LogP: | 1.85660 |
1-(3,4-dimethoxy-phenyl)-2-methylamino-ethanone; hydrochloride
A
N-methylhomoveratrylamine
B
1-(3,4-dimethoxyphenyl)-2-(methylamino)ethan-1-ol
Conditions | Yield |
---|---|
Stage #1: 1-(3,4-dimethoxy-phenyl)-2-methylamino-ethanone; hydrochloride With hydrogen; 5%-palladium/activated carbon In water at 75℃; under 2585.81 Torr; for 16 - 40h; Stage #2: With sodium hydroxide In water; toluene pH=12; Product distribution / selectivity; | A n/a B 95.1% |
N-[2-(3,4-dimethoxyphenyl)ethyl]formamide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With sodium tetrahydroborate; boron trifluoride diethyl etherate In tetrahydrofuran 1) room temperature, 1 h; 2) reflux, 3 h; | 90% |
With tetrahydrofuran; lithium aluminium tetrahydride | |
With lithium aluminium tetrahydride In tetrahydrofuran; diethyl ether |
methanesulphonic acid,2-(3,4-dimethoxyphenyl)ethyl ester
methylamine
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
Stage #1: methanesulphonic acid,2-(3,4-dimethoxyphenyl)ethyl ester; methylamine In methanol; water at 140℃; under 15514.9 Torr; for 0.166667h; Flow reactor; Stage #2: With potassium hydroxide In water | 90% |
N-[2-(3,4-dimethoxyphenyl)ethyl]-2,2,2-trifluoroacetamide
methyl iodide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With sodium hydride In tetrahydrofuran for 4h; Ambient temperature; | 82% |
3,4-dimethoxystyrene
N-methylhydroxylamine-O-sulphonic acid
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
Stage #1: 3,4-dimethoxystyrene With Schwartz's reagent In tetrahydrofuran at 25℃; Stage #2: N-methylhydroxylamine-O-sulphonic acid In tetrahydrofuran at 50℃; for 0.5h; | 71% |
Conditions | Yield |
---|---|
Stage #1: 2-(3,4-dimethoxyphenyl)-ethylchloride; methylamine In ethanol at 20℃; for 1h; Stage #2: With triisobutylaluminum In ethanol at 60℃; for 32h; | 68% |
(3,4-dimethoxy-phenyl)-thioacetic acid methylamide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With hydrogenchloride an Blei-Elektroden; |
benzaldehyde
2-(3,4-dimethoxyphenyl)-ethylamine
dimethyl sulfate
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
With benzene und Erwaermen des Reaktionsprodukts mit wss.Aethanol; |
benzaldehyde
2-(3,4-dimethoxyphenyl)-ethylamine
methyl iodide
N-methylhomoveratrylamine
Conditions | Yield |
---|---|
und Erwaermen des Reaktionsprodukts mit wss.Aethanol; |
Conditions | Yield |
---|---|
With palladium; benzene Hydrogenation; |