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365564-11-0

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CAS No.: 365564-11-0
Name: 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)-1H-pyrrole
Article Data: 26
Molecular Structure:
Molecular Structure of 365564-11-0 (3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)-1H-pyrrole)
Formula: C19H36BNO2Si
Molecular Weight: 349.397
Synonyms: 3-(4,4,5,5-Tetramethyl-1,3,2-dioxaborolan-2-yl)-1-[tris(1-methylethyl)silyl]-1H-pyrrole;tri(propan-2-yl)-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)pyrrol-1-yl]silane;
Density: 0.941g/cm3
Melting Point: 59 °C
Boiling Point: 383.588oC at 760 mmHg
Flash Point: 185.788oC
PSA: 23.39000
LogP: 4.81090
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365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
With 1-(2-borylphenyl)-2,2,6,6-tetramethylpiperidine dimer In chloroform at 80℃; for 16h;98%
With Cp*Rh(η4-C6Me6) In cyclohexane at 150℃; for 41h;81%
Stage #1: N-triisopropylsilylpyrrole With 2,6-dimethylpyridine; aluminum (III) chloride; boron trichloride In n-heptane; dichloromethane at 20℃; for 16h; Inert atmosphere;
Stage #2: 4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane With triethylamine In n-heptane; dichloromethane for 0.25h; Inert atmosphere;		52%
With poly((2-(piperidin-1-ium-1-yl)-5-vinylphenyl)trifluoroborate) In chloroform-d1 at 90℃; for 16h; Reagent/catalyst; Inert atmosphere; Glovebox; Sealed tube;
76-09-5

2,3-dimethyl-2,3-butane diol

C6Cl4O2BN(C2H5)3(1+)*AlCl4(1-)=C6Cl4O2BN(C2H5)3[AlCl4]

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N-triisopropylsilylpyrrole

365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
With Et3N In dichloromethane byproducts: Et3NH-AlCl4; to borenium cation made in situ (in Schlenk, to soln. Et2N (CH2Cl2) added Cl4CatBCl, AlCl3; stirred) at 20°C arene added (CH2Cl2); excessEt3N added; pinacol added; stirred for 32 h;; (11)B (1H) NMR; volatiless remowed under vac; extracted (hexane); filtered through silica; removal of solvent;;95%
...Expand
76-09-5

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365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
With triethylamine In dichloromethane for 3h;90%
With triethylamine In toluene at 20℃; for 1h; Schlenk technique;45%
With triethylamine In dichloromethane for 1h; Inert atmosphere;101 mg
With triethylamine at 0 - 20℃; for 1h; Inert atmosphere;
With triethylamine In 1,2-dichloro-ethane at 20℃; Schlenk technique; Inert atmosphere;
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2,3-dimethyl-2,3-butane diol

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365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
With triethylamine at 20℃; for 0.5h;90%
76-09-5

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N-triisopropylsilylpyrrole

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boron trichloride

365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
With AlCl3; 2,6-lutidine In dichloromethane 1:1 mixt. of BCl3 and AlCl, pinacol (2.3-3.0 equiv.) and lutidine (15 equiv.) for 14 h;90%
...Expand
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N-triisopropylsilylpyrrole

365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
Stage #1: N-triisopropylsilylpyrrole With 2,6-dimethylpyridine; aluminum (III) chloride; boron trichloride In n-heptane; dichloromethane at 20℃; for 14h; Inert atmosphere;
Stage #2: 2,3-dimethyl-2,3-butane diol With triethylamine In n-heptane; dichloromethane at 20℃; for 0.5h; Inert atmosphere;		90%
76-09-5

2,3-dimethyl-2,3-butane diol

C6H4O2BN(C2H5)3(1+)*AlCl4(1-)=C6H4O2BN(C2H5)3[AlCl4]

87630-35-1

N-triisopropylsilylpyrrole

365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
With Et3N In dichloromethane byproducts: Et3NH-AlCl4; to borenium cation made in situ (in Schlenk, to soln. Et2N (CH2Cl2) added CatBCl, AlCl3; stirred) at 20°C arene added (CH2Cl2); excess Et3N added; pinacol added; stirred for 32 h;; (11)B (1H) NMR; volatiless remowed under vac; extracted (hexane); filtered through silica; removal of solvent;;89%
...Expand
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4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; triethylamine; dichloro bis(acetonitrile) palladium(II) In toluene at 90℃; for 18h;85%
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; triethylamine; dichloro bis(acetonitrile) palladium(II) In toluene at 90℃; for 18h;85%
With dichloro bis(acetonitrile) palladium(II); triethylamine In toluene 1.2 equiv. pinacol borane react. catalyzed by 3% (PdCl2(CH3CN)2), 9% dialkylmonophosphino biaryl (toluene) at 90°C;79%
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3-iodo-1-(triisopropylsilyl)-1H-pyrrole

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4,4,5,5-tetramethyl-[1,3,2]-dioxaboralane

365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); triethylamine In toluene at 20 - 90℃; Inert atmosphere;80%
With dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; dichloro bis(acetonitrile) palladium(II); triethylamine In toluene
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bis(pinacol)diborane

365564-11-0

3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)pyrrole

Conditions
ConditionsYield
bis(1,5-cyclooctadiene)diiridium(I) dichloride; 4,4'-di-tert-butyl-2,2'-bipyridine In octane at 80℃; for 16h;79%
With [IrCl(COD)]2 In octane at 80℃; for 48h; Inert atmosphere;77%
With 4,4'-di-tert-butyl-2,2'-bipyridine; bis(1,5-cyclooctadiene)diiridium(I) dichloride In hexane at 100℃; for 0.833333h; microwave irradiation;
With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4′-di-(tert-butyl)-2,2′-bipyridyl In tetrahydrofuran at 80℃; for 24h; High pressure; Inert atmosphere; regioselective reaction;
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  • 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)-1H-pyrrole

  • Casno:

    365564-11-0

    3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-(triisopropylsilyl)-1H-pyrrole

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    At Capot,We can synthesize and purify your complex molecules from 100 gram to 10 tons.Appearance:Clear colorless to light yellow liquid Storage:Dry,Seal and Cool place Package:1G,5G,10G,25G,100G,250G,500G,1KG,5KG,10KG,25KG,50KG,100KG,150KG,200KG. App

    Welcome to Capot . Established in 1996 ,Capot Chemical Co.,Ltd is a fine organics manufacturing facility which located in Hangzhou,P.R.China. We produce a wide range of organics,

  • Capot Chemical Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-571-85586718

    Address:join hands science park,NO.4028 nanhuan road,hanghzou ,zhejiang,china

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  • 1H-Pyrrole,3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-[tris(1-methylethyl)silyl]-

  • Casno:

    365564-11-0

    1H-Pyrrole,3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-[tris(1-methylethyl)silyl]-

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Shanghai, Run-Biotech Co., Ltd is a leading domestic pharmaceutical, biopharmaceutical, and health care products R & D outsourcing services company. As an innovation-driven and customer-focused company, Run Biotech provides a broad and integrated por

    Shanghai fine pharma co., Ltd. is a professional enterprise with chemical reagents and fine chemical products development, development and trade. The company has a sound research a

  • Shanghai Run-Biotech Co., Ltd.

     China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+86-21-31576854/57171705 / 57171706

    Address:second floor, building 3, No.999, jiangyue Road, minghang District, Shanghai, China

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  • 1-TRIISOPROPYLSILANYL-1H-PYRROLE-3-BORONIC ACID PINACOL ESTER

  • Casno:

    365564-11-0

    1-TRIISOPROPYLSILANYL-1H-PYRROLE-3-BORONIC ACID PINACOL ESTER

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Known for its best quality and competitve price, this chemicals we offered is widely appreciated by our customers.Appearance:yellow to white solid Storage:keep sealed and keep from direct light Package:According client's requirements Application:Phar

    Jinan YSPharma Biotechnology Co., Ltd is a large group specializing in contract manufacturing to the pharmaceutical, agrochemical and Fine chemicals with top quality products and s

  • coolpharm Ltd

    China (Mainland)  |  Contact Details

    Business Type:Other

    Tel:86-531-8233381 86-18678657237

    Address:Room 302,Building 1,Union Fortune Square, No. 2117,Tianchen Road,High-tech Zone,Jinan,Shandong,China

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  • 1-(triisopropylsilyl)-1H-pyrrol-3-ylboronic acid pinacol ester

  • Casno:

    365564-11-0

    1-(triisopropylsilyl)-1H-pyrrol-3-ylboronic acid pinacol ester

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four yearsOur key scientific leadership team has gained experience in top research and developmen

    Debyesci is here who supplied several kinds of chemical products to global pharmaceutical, drug discovery, agrochemical and biotechnology industries for four years Our key scienti

  • Debye Scientific

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+85221376140

    Address:Rm. 19C, Lockhart Ctr., 301-307 Lockhart Rd., Wan Chai

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  • 1H-Pyrrole, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-[tris(1-methylethyl)silyl] -

  • Casno:

    365564-11-0

    1H-Pyrrole, 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1-[tris(1-methylethyl)silyl] -

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    YUYONGMEI was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu Province with 1200 square meters’ R&D center. Our R&D center has a well-equipped synthetic laboratory a

    YUYONGMEI was established in Aug,1999, located in the industrial park of Nanjing University of Technology, It is a private enterprises in Jiangsu Province with 1200 square meters’

  • yuyongmei

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:.+86-571-12345678

    Address:sichuan

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