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CAS No.: | 3844-53-9 |
---|---|
Name: | Ethyl 2,6-diaminohexanoate dihydrochloride |
Article Data: | 5 |
Molecular Structure: | |
Formula: | C8H18 N2 O2 . 2 Cl H |
Molecular Weight: | 247.165 |
Synonyms: | L-Lysine,ethyl ester, dihydrochloride (9CI); Lysine, ethyl ester, dihydrochloride, L-(7CI,8CI); Lysine ethyl ester dihydrochloride; NSC 162742 |
EINECS: | 223-340-3 |
Density: | g/cm3 |
Melting Point: | ~150 °C (dec.) |
Boiling Point: | 261.9 °C at 760 mmHg |
Flash Point: | 97.3 °C |
Appearance: | White Powder |
Hazard Symbols: | 36/37/38:; |
Risk Codes: | 36/37/38 |
Safety: | 22-24/25 |
PSA: | 78.34000 |
LogP: | 3.01040 |
ethanol
L-Lysine hydrochloride
L-lysine ethyl ester dihydrochloride
Conditions | Yield |
---|---|
With thionyl chloride Reflux; | 87% |
With thionyl chloride at -10℃; for 6h; Reflux; | 87% |
With hydrogenchloride at 70℃; for 5h; |
Conditions | Yield |
---|---|
With hydrogenchloride |
Conditions | Yield |
---|---|
Stage #1: C11H15N2O5PolS With benzotriazol-1-ol; dicyclohexyl-carbodiimide In dichloromethane at 20℃; for 3h; Stage #2: L-lysine ethyl ester dihydrochloride With dmap In dichloromethane at 20℃; for 42h; | 94% |
Conditions | Yield |
---|---|
With triethylamine In dichloromethane at 20℃; for 6h; | 88.8% |
Conditions | Yield |
---|---|
With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide at 20℃; for 16h; Inert atmosphere; | 85% |
Conditions | Yield |
---|---|
With pyridine; acetic acid at 20℃; for 6h; Reflux; | 79% |
With pyridine; acetic acid for 8h; Reflux; |
2-(2-methoxyethoxy)acetic acid
L-lysine ethyl ester dihydrochloride
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate In N,N-dimethyl-formamide at 20℃; Cooling with ice; | 77.8% |
L-lysine ethyl ester dihydrochloride
geldanmycin
Conditions | Yield |
---|---|
With triethylamine In tetrahydrofuran; methanol at 60℃; | 74.1% |
Conditions | Yield |
---|---|
Stage #1: 2-methyl-5-nitroimidazole-1-acetic acid With 1,1'-carbonyldiimidazole In N,N-dimethyl-formamide for 0.25h; Inert atmosphere; Stage #2: L-lysine ethyl ester dihydrochloride With triethylamine In N,N-dimethyl-formamide Inert atmosphere; | 69% |
Conditions | Yield |
---|---|
With triethylamine In N,N-dimethyl-formamide at 20℃; | 66% |
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