Name: 4-HYDROXYBENZOIC ACID N-NONYL ESTER
SKU: 38713-56-3

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Pharmaceutical (13)
Organic Chemicals (6)

Basic Information

CAS No.:

38713-56-3

Name:

4-HYDROXYBENZOIC ACID N-NONYL ESTER

Article Data:

Molecular Structure:

Formula:

C16H24 O3

Molecular Weight:

264.365

Synonyms:

Benzoicacid, p-hydroxy-, nonyl ester (7CI); 4-Hydroxy nonylbenzoate; Nonyl4-hydroxybenzoate; Nonyl p-hydroxybenzoate; n-Nonyl 4-hydroxybenzoate;p-Hydroxybenzoic acid nonyl ester

Density:

1.025g/cm³

Melting Point:

44°C

Boiling Point:

382.4°Cat760mmHg

Flash Point:

152°C

Solubility:

1.275g/L(25 oC)

Risk Codes:

36/37/38

Safety:

Risk Statements	36/37/38
Safety Statements	26-36/37/39

PSA:

46.53000

LogP:

4.29960

Synthetic route

: 134447-10-2
4-Methoxycarbonyloxy-benzoic acid nonyl ester

: 38713-56-3
n-nonyl 4-hydroxybenzoate

Conditions

Conditions	Yield
With ammonium hydroxide In ethanol for 1h; Ambient temperature;	82.6%

: 1486-51-7
p-(benzyloxy)benzoic acid

: 38713-56-3
n-nonyl 4-hydroxybenzoate

Conditions

Conditions	Yield
With hydrogen; palladium on activated charcoal In ethanol at 40℃; under 2585.7 Torr; for 2h;	82.5%
Multi-step reaction with 2 steps 1: Ph3P; diisopropyl azodicarboxylate / tetrahydrofuran / 2 h / 20 °C 2: H2; AcOH / Pd(OH)2/C / ethyl acetate / 12 h View Scheme
Multi-step reaction with 2 steps 1: PPh3; diisopropyl azodicarboxylate / tetrahydrofuran / 20 °C 2: H2; AcOH / Pd(OH)2/C / ethyl acetate View Scheme
Multi-step reaction with 2 steps 1: 34 percent / benzene; dimethylformamide 2: 65.4 percent / H2 / hydrogenation catalyst View Scheme

: 134447-07-7
Nonyl 4-benzyloxybenzoate

: 38713-56-3
n-nonyl 4-hydroxybenzoate

Conditions

Conditions	Yield
With hydrogen; hydrogenation catalyst	65.4%
With hydrogen; acetic acid; palladium dihydroxide In ethyl acetate
With hydrogen; acetic acid; palladium dihydroxide In ethyl acetate for 12h;

: 143-08-8
nonyl alcohol

: 99-96-7
4-hydroxy-benzoic acid

: 38713-56-3
n-nonyl 4-hydroxybenzoate

Conditions

Conditions	Yield
With dicyclohexyl-carbodiimide In tetrahydrofuran for 20h;	64%
With sulfuric acid In toluene for 4h; Heating;	24.8%
With hydrogenchloride

: 143-08-8
nonyl alcohol

: 38713-56-3
n-nonyl 4-hydroxybenzoate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: Ph3P; diisopropyl azodicarboxylate / tetrahydrofuran / 2 h / 20 °C 2: H2; AcOH / Pd(OH)2/C / ethyl acetate / 12 h View Scheme
Multi-step reaction with 2 steps 1: PPh3; diisopropyl azodicarboxylate / tetrahydrofuran / 20 °C 2: H2; AcOH / Pd(OH)2/C / ethyl acetate View Scheme
Multi-step reaction with 2 steps 1: 1) SOCl2, 2) Et3N / 2) CH2Cl2 2: 82.6 percent / conc. NH4OH / ethanol / 1 h / Ambient temperature View Scheme

: 32122-11-5
4-benzyloxy-benzoic acid methyl ester

: 38713-56-3
n-nonyl 4-hydroxybenzoate

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: base / tetrahydrofuran; aq. ethanol / 24 h / Heating 2: 34 percent / benzene; dimethylformamide 3: 65.4 percent / H2 / hydrogenation catalyst View Scheme

: 99-76-3
methyl 4-hydroxylbenzoate

: 38713-56-3
n-nonyl 4-hydroxybenzoate

Conditions

Conditions	Yield
Multi-step reaction with 4 steps 1: benzene; dimethylformamide 2: base / tetrahydrofuran; aq. ethanol / 24 h / Heating 3: 34 percent / benzene; dimethylformamide 4: 65.4 percent / H2 / hydrogenation catalyst View Scheme

: 14180-11-1
4-(methoxycarbonyloxy)benzoic acid

: 38713-56-3
n-nonyl 4-hydroxybenzoate

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 1) SOCl2, 2) Et3N / 2) CH2Cl2 2: 82.6 percent / conc. NH4OH / ethanol / 1 h / Ambient temperature View Scheme

: 28141-24-4
4-hydroxybenzoyl chloride

: 143-08-8
nonyl alcohol

: 38713-56-3
n-nonyl 4-hydroxybenzoate

Conditions

Conditions	Yield
With sulfuric acid In 1,1-dichloroethane

: 38713-56-3
n-nonyl 4-hydroxybenzoate

: nonyl 4-[(aminosulphonyl)oxy]benzoate

Conditions

Conditions	Yield
With sulphamoyl chloride; sodium hydride In N,N-dimethyl-formamide; toluene for 10h; Heating;	10.7%
Stage #1: n-nonyl 4-hydroxybenzoate With sodium hydride In N,N-dimethyl-formamide at 0℃; Stage #2: With sulphamoyl chloride In N,N-dimethyl-formamide; toluene
Stage #1: n-nonyl 4-hydroxybenzoate With sodium hydride In N,N-dimethyl-formamide at 0℃; for 0.5h; Stage #2: With sulphamoyl chloride In N,N-dimethyl-formamide; toluene for 10h;