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3919-74-2

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CAS No.: 3919-74-2
Name: 3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylic acid
Article Data: 13
Molecular Structure:
Molecular Structure of 3919-74-2 (3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylic acid)
Formula: C11H7ClFNO3
Molecular Weight: 255.633
Synonyms: 3-(2-CHLORO-6-FLUOROPHENYL)-5-METHYLISOXAZOLE-4-CARBOXYLIC ACID;LABOTEST-BB LT00454096;RARECHEM AL BO 0550;3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carbonitrile-4-carboxylicacid;3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylic acid 97%;3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylicacid97%;3-(2-CHLORO-6-FLUOROPHENYL)-5-METHYLISOXAZOLE-4-CARBOXYLIC A;3-(2-Chloro-6-fluorophenyl)-5-methyl-4-isoxazolecarboxic Acid
EINECS: 223-486-8
Density: 1.454 g/cm3
Melting Point: 202 °C
Boiling Point: 360.7 °C at 760 mmHg
Flash Point: 171.9 °C
Hazard Symbols: IrritantXi
Risk Codes: 36/37/38
Safety: 26-36/37/39-37/39-36
PSA: 63.33000
LogP: 3.14070
Related products
Synthetic route
1239346-71-4

(3-(2-chloro-6-fluorophenyl)-5-methylisoxazol-4-yl)methanol

3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

Conditions
ConditionsYield
Stage #1: (3-(2-chloro-6-fluorophenyl)-5-methylisoxazol-4-yl)methanol With potassium permanganate; disodium hydrogenphosphate In methanol; water at 25℃; Continuous flow conditions; Sonication;
Stage #2: With hydrogenchloride; sodium thiosulfate; sodium chloride In methanol; water; ethyl acetate		87%
51088-25-6

2-chloro-6-fluoro-N-hydroxybenzene-1-carbonimidoyl chloride

105-45-3

acetoacetic acid methyl ester

3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

Conditions
ConditionsYield
With ethanol; triethylamine at 5℃;72%
4415-09-2

methyl 3-(2-chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylate

3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

Conditions
ConditionsYield
With potassium hydroxide In ethanol
With water; sodium hydroxide In methanol for 1h; pH=11 - 13; Reflux;
With water; sodium hydroxide In ethanol at 60℃; for 24h;
With sodium hydroxide In water for 3h;
387-45-1

2-chloro-6-fluorobenzaldehyde

3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: (i) NH2OH, (ii) Cl2, CHCl3, (iii) /BRN= 506727/, MeOH
2: aq. KOH / ethanol
View Scheme
Multi-step reaction with 4 steps
1.1: hydroxylamine sulfate / methanol / 0.5 h
1.2: 0.5 h / pH 8 - 9 / Reflux
2.1: chlorine / methanol / 0 - 5 °C
3.1: sodium hydroxide / methanol / 0.5 h / 0 - 5 °C / pH 10
3.2: 2 h / 0 - 20 °C / pH 9
4.1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux
View Scheme
Multi-step reaction with 3 steps
1: sodium carbonate; hydroxylamine hydrochloride / ethanol; water / 2 h / 20 °C
2: pyridine; N-chloro-succinimide / chloroform / 1.5 h / 20 °C
3: ethanol; triethylamine / 5 °C
View Scheme
51088-25-6

2-chloro-6-fluoro-N-hydroxybenzene-1-carbonimidoyl chloride

3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: sodium hydroxide / methanol / 0.5 h / 0 - 5 °C / pH 10
1.2: 2 h / 0 - 20 °C / pH 9
2.1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux
View Scheme
443-33-4

N-[(2-chloro-6-fluorophenyl)methylidene]hydroxylamine

3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: chlorine / methanol / 0 - 5 °C
2.1: sodium hydroxide / methanol / 0.5 h / 0 - 5 °C / pH 10
2.2: 2 h / 0 - 20 °C / pH 9
3.1: water; sodium hydroxide / methanol / 1 h / pH 11 - 13 / Reflux
View Scheme
Multi-step reaction with 2 steps
1: pyridine; N-chloro-succinimide / chloroform / 1.5 h / 20 °C
2: ethanol; triethylamine / 5 °C
View Scheme
387-45-1

2-chloro-6-fluorobenzaldehyde

105-45-3

acetoacetic acid methyl ester

3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

Conditions
ConditionsYield
Stage #1: 2-chloro-6-fluorobenzaldehyde With hydroxylamine sulfate In methanol at 20 - 40℃; for 1h;
Stage #2: With chlorine; sodium carbonate; triethylamine In methanol at 0 - 20℃; for 24h; pH=~ 9.5; Inert atmosphere;
Stage #3: acetoacetic acid methyl ester With sodium carbonate In methanol pH=~ 7 - 7.5;
83817-51-0

ethyl 3-(2-chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylate

3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

Conditions
ConditionsYield
With water; sodium hydroxide In ethanol at 60℃; for 24h;
5250-39-5, 24223-74-3

floxacillin

A

124-38-9

carbon dioxide

B

5,5-dimethyl-thiazolidine-2,4-dicarboxlic acid

C

3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

Conditions
ConditionsYield
With potassium tellurite; sulfuric acid at 14.84℃; Kinetics; Thermodynamic data; Temperature;
...Expand
3919-74-2

3-(2-chloro-6-flourophenyl)-5-methyl-isoxazole-4-carboxylic acid

3-(2-chloro-6-fluorophenyl)-5-methylisoxazole-4-carbonyl chloride

Conditions
ConditionsYield
With phosphorus pentachloride at 45℃; for 1h;88%
With phosphorus pentachloride In toluene
With phosphorus pentachloride In toluene
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  • 3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylic acid

  • Casno:

    3919-74-2

    3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylic acid

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    factory?direct?saleAppearance:White powder Storage:Sealed and preserved Package:200/Kilograms Application:healing drugs Transportation:By sea Port:Shanghai/tianjin

    Henan Kanbei Chemical Co., Ltd. is a modern high-tech chemical enterprise integrating R&D, production and sales. The company has strong technical strength, advanced equipment, stri

  •  Henan Kanbei Chemical Co.,LTD

    China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:86-152-37804566

    Address:Evergrande Future City, intersection of Zhengkai Avenue and Sixteenth Street, Kaifeng Area, Henan Pilot Free Trade Zone

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  • 3919-74-2

  • Casno:

    3919-74-2

    3919-74-2

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    Good Quality Package:1kg/bag Application:Medical or chemical Transportation:Air/Train/Sea Port:Shenzhen

    Shanghai Chinqesen Biotechnology Co., Ltd. Company slogan:?Innovation, cooperation and win-win Company introduction:?Shanghai Chinqesen Biotechnology Co., Ltd. is a professional ph

  •  Shanghai Chinqesen Biotechnology Co., Ltd.

    China (Mainland)  |  Contact Details

    Business Type:Trading Company

    Tel:+8617316470195

    Address:333 Songze Avenue, Qingpu District, Shanghai

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  • 3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylic acid 3919-74-2

  • Casno:

    3919-74-2

    3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylic acid 3919-74-2

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

    high purity lowest priceAppearance:solid or liquid Storage:in sealed air resistant place Package:Foil bag; Drum; Plastic bottle Application:Pharma;Industry;Agricultural Transportation:by sea or air Port:any port in China

    Shenzhen Foris Technology Co.LTD is located in Shenzhen ，Guangdong， is the leading supplier for electronic chemicals,APIs, pharmaceutical intermediates, fine chemicals which can be

  •  Shenzhen Foris Technology Co. LTD

     China (Mainland)  |  Contact Details

    Business Type:Lab/Research institutions

    Tel:+86 15889746615

    Address:BuildingA7, KingloryTongxin International Industry Park, Wanglei Avenue, Hi-tec District

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Chemistry

Product Name:3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylic acid
CAS No:3919-74-2
Synonyms:3-(2-CHLORO-6-FLUOROPHENYL)-5-METHYLISOXAZOLE-4-CARBOXYLIC ACID;LABOTEST-BB LT00454096;RARECHEM AL BO 0550;3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carbonitrile-4-carboxylicacid;3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylic acid 97%;3-(2-Chloro-6-fluorophenyl)-5-methylisoxazole-4-carboxylicacid97%;3-(2-CHLORO-6-FLUOROPHENYL)-5-METHYLISOXAZOLE-4-CARBOXYLIC A;3-(2-Chloro-6-fluorophenyl)-5-methyl-4-isoxazolecarboxic Acid
Molecular Formula:C11H7ClFNO3
Formula Weight:255.63
Melting Point:202 °C
Molecular Structure:

Safety Profile

Hazard Codes  Xi
Risk Statements  36/37/38-37/38-36
Safety Statements  26-36/37/39-37/39-36
Hazard Note  Irritant