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4352-30-1

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Basic Information
CAS No.: 4352-30-1
Name: CYCLOHEXYL-METHANESULFONYL CHLORIDE
Article Data: 12
Molecular Structure:
Molecular Structure of 4352-30-1 (CYCLOHEXYL-METHANESULFONYL CHLORIDE)
Formula: C7H13ClO2S
Molecular Weight: 196.698
Synonyms: Cyclohexyl-methansulfonylchlorid;cyclohexylmethyl sulfonyl chloride;Cyclohexylmethanesulphonyl chloride;Cyclohexyl-methanesulfonyl chloride;CZS-60-0;
Density: 1.229
Melting Point: 114-115oC
Boiling Point: 280oC
Flash Point: 123oC
Risk Codes: R34
PSA: 42.52000
LogP: 3.21610
Related products
Synthetic route
107512-01-6

S-(cyclohexylmethyl) ethanethioate

4352-30-1

cyclohexylmethylsulfonyl chloride

Conditions
ConditionsYield
With hydrogenchloride; N-chloro-succinimide In water; acetonitrile at 0 - 20℃; Inert atmosphere;100%
4352-27-6

cyclohexylmethanesulfonic acid

4352-30-1

cyclohexylmethylsulfonyl chloride

Conditions
ConditionsYield
With oxalyl dichloride; N,N-dimethyl-formamide In dichloromethane at -20 - 20℃; for 2.5h;19%
17356-08-0

thiourea

2550-36-9

(bromomethylcyclohexane)

4352-30-1

cyclohexylmethylsulfonyl chloride

Conditions
ConditionsYield
With ethanol Behandeln des Reaktionsprodukts mit wss.NaOH und anschliessend mit Chlor und wss.Essigsaeure;

cyclohexylmethylsulfonate sodium salt

4352-30-1

cyclohexylmethylsulfonyl chloride

Conditions
ConditionsYield
With thionyl chloride; N,N-dimethyl-formamide for 12h; Heating;
With trichlorophosphate
With trichlorophosphate
1072-95-3

cyclohexylmethyl chloride

4352-30-1

cyclohexylmethylsulfonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: Na2SO3 / 1,2-dimethoxy-ethane; H2O / 24 h / Heating
2: SOCl2, DMF / 12 h / Heating
View Scheme

(S)-5-(cyclohexylmethyl)sulfanylmethyl-5-methylimidazolidine-2,4-dione

A

1206882-48-5

(S)-5-methyl-5-trichloromethylimidazolidine-2,4-dione

B

4352-30-1

cyclohexylmethylsulfonyl chloride

Conditions
ConditionsYield
With water; chlorine In acetic acid Mechanism; Reagent/catalyst;A 41 mg
B n/a
2550-36-9

(bromomethylcyclohexane)

4352-30-1

cyclohexylmethylsulfonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: sodium hydrogensulfite / water
2: trichlorophosphate
View Scheme
Multi-step reaction with 2 steps
1: sodium sulfite / water; acetone / 16 h / 90 °C
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 2.5 h / -20 - 20 °C
View Scheme
100-49-2

cyclohexylmethyl alcohol

4352-30-1

cyclohexylmethylsulfonyl chloride

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: triethylamine / dichloromethane / 6 h / 0 - 20 °C / Inert atmosphere
2: N,N-dimethyl-formamide / 5 h / 60 °C / Inert atmosphere
3: hydrogenchloride; N-chloro-succinimide / acetonitrile; water / 0 - 20 °C / Inert atmosphere
View Scheme
2550-36-9

(bromomethylcyclohexane)

A

4352-30-1

cyclohexylmethylsulfonyl chloride

B

C7H13BrO2S

Conditions
ConditionsYield
Stage #1: Cyclohexylmethyl bromide With thiourea In ethanol for 36h; Reflux;
Stage #2: With hydrogenchloride; N-chloro-succinimide In water; acetonitrile at 10℃; for 0.5h;
4352-30-1

cyclohexylmethylsulfonyl chloride

125125-38-4, 125125-40-8

2,3-Dicyclohexylthiiran-1,1-dioxid

Conditions
ConditionsYield
With triethylamine In acetonitrile at -40℃;91%
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