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CAS No.: | 491-11-2 |
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Name: | 3-chloro-4-nitrophenol |
Article Data: | 32 |
Molecular Structure: | |
Formula: | C6H4ClNO3 |
Molecular Weight: | 173.556 |
Synonyms: | Phenol, 3-chloro-4-nitro-;3-chloro-4-nitro-phenol;EINECS 207-730-0;2-Chloro-4-hydroxynitrobenzene;4-nitro-3-chlorophenol;Phenol,3-chloro-4-nitro;3-Chlor-4-nitro-phenol;3-Chlor-4-nitro-1-hydroxy-benzol; |
Density: | 1.554g/cm3 |
Melting Point: | 120-121℃ |
Boiling Point: | 330.5°Cat760mmHg |
Flash Point: | 153.7°C |
PSA: | 66.05000 |
LogP: | 2.47700 |
Conditions | Yield |
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With tetrabutylammonium chromate; sodium nitrite In dichloromethane for 69h; Reflux; chemoselective reaction; | 98% |
With copper(II) nitrate trihydrate In tetrahydrofuran at 50℃; for 4h; regiospecific reaction; | 90% |
With potassium hydrogensulfate; sodium perborate hexahydrate; sodium nitrite In neat (no solvent) for 0.0277778h; Molecular sieve; Microwave irradiation; regioselective reaction; | 75% |
3-chloro-4-nitroanisole
3-chloro-4-nitrophenol
Conditions | Yield |
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With potassium hydroxide at 110℃; for 15h; | 90.5% |
Conditions | Yield |
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With potassium hydroxide In water at 150℃; for 4h; Reagent/catalyst; Time; Inert atmosphere; Sealed tube; | 82.1% |
3-chloro-4-nitroaniline
A
2-hydroxy-4-amino-1-nitrobenzene
B
3-chloro-4-nitrophenol
C
4-nitroresorcinol
Conditions | Yield |
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With water; sodium hydroxide at 100℃; for 50h; | A 22% B 72% C 5% |
Conditions | Yield |
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With nitric acid; acetic acid at -20℃; for 2.5h; Inert atmosphere; | A 20% B 43% |
With sodium nitrate; sulfuric acid In water at 25℃; for 4h; | A n/a B 20% |
With nitric acid |
Conditions | Yield |
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With Cumene hydroperoxide; potassium tert-butylate In ammonia at -33℃; | A 37% B 37% |
3-chloro-4-nitrosophenol
3-chloro-4-nitrophenol
Conditions | Yield |
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With sodium hydroxide; potassium hexacyanoferrate(III) | |
With potassium hexacyanoferrate(III) Yield given; |
tris(3-chlorophenyl) phosphate
3-chloro-4-nitrophenol
Conditions | Yield |
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With sulfuric acid; nitric acid anschliessendes Erhitzen mit Wasser; | |
With sulfuric acid; nitric acid anschliessendes Erhitzen mit Wasser; |
2-Chloronitrobenzene
A
3-chloro-4-nitrophenol
B
2-nitro-3-chlorophenol
C
2-hydroxynitrobenzene
Conditions | Yield |
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With potassium hydroxide; oxygen In ammonia at -33℃; | A 0.48 g B 1.01 g C 0.39 g |
Conditions | Yield |
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In benzonitrile at 25℃; Equilibrium constant; ionic strength 0.1 M, var. solv.; |