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5090-29-9

Basic Information
CAS No.: 5090-29-9
Name: 3,4-dihydroxy-α-aminoacetophenone hydrochloride
Molecular Structure:
Molecular Structure of 5090-29-9 (3,4-dihydroxy-α-aminoacetophenone hydrochloride)
Formula: C8H9NO3
Molecular Weight: 203.625
Synonyms: Noradenalone hydrochloride;Noradrenalone Hydrochloride;
Density: 1.375g/cm3
Melting Point: 255 °C
Boiling Point: 435.1°Cat760mmHg
Flash Point: 217°C
PSA: 83.55000
LogP: 1.74150
Synthetic route
5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

55-27-6

norepinephrine hydrochloride

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol at 45℃; under 0.30003 - 0.375038 Torr; for 5h; Temperature; Pressure; Time;96.7%
5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

S-(-)-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeuredichlorid

104819-55-8, 104873-27-0, 104873-28-1

S-(-)-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeure-di-N,N'-1-(3,4-dihydroxyphenyl)-1-oxo-2-amido-ethan

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; benzene for 30h;64.3%
5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

R-(+)-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeuredichlorid

104819-55-8, 104873-27-0, 104873-28-1

R-(+)-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeure-di-N,N'-1-(3,4-dihydroxyphenyl)-1-oxo-2-amido-ethan

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; benzene for 30h;61.4%
941301-17-3, 941301-22-0, 104819-54-7, 104873-26-9, 104873-34-9

R,S-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeuredichlorid

5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

104819-55-8, 104873-27-0, 104873-28-1

R,S-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeure-di-N,N'-1-(3,4-dihydroxyphenyl)-1-oxo-2-amido-ethan

Conditions
ConditionsYield
With sodium hydrogencarbonate In water; benzene for 30h;58.5%
5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

A

80098-03-9

noradrenalone-3-O-sulfate

B

80098-04-0

noradrenalone-4-O-sulfate

Conditions
ConditionsYield
With chlorosulfonic acid at -45 - -2℃; for 1h; Yield given;
5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

112346-92-6

dl-norepinephrine-3-O-sulfate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chlorosulfonic acid / 1 h / -45 - -2 °C
2: NaBH4 / methanol; propan-2-ol / 7 h
View Scheme
5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

35538-87-5

dl-norepinephrine-4-O-sulfate

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: chlorosulfonic acid / 1 h / -45 - -2 °C
2: NaBH4 / methanol; propan-2-ol / 7 h
View Scheme
5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

138-65-8

Norepinephrine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 58.5 percent / NaHCO3 / benzene; H2O / 30 h
2: 74 percent / NaBH4 / methanol / 24 h
3: 51.4 percent / H2, conc HCl / Pd/C / ethanol / 6 h / Ambient temperature
View Scheme
5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

51-41-2

norepinephrine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 61.4 percent / NaHCO3 / benzene; H2O / 30 h
2: NaBH4 / methanol / 24 h
3: 51.4 percent / H2, conc HCl / Pd/C / ethanol / 6 h / Ambient temperature
View Scheme
5090-29-9

1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid

149-95-1

D-noradrenaline

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1: 64.3 percent / NaHCO3 / benzene; H2O / 30 h
2: NaBH4 / methanol / 24 h
3: 54.2 percent / H2, conc HCl / Pd/C / ethanol / 6 h / Ambient temperature
View Scheme
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    3,4-dihydroxy-α-aminoacetophenone hydrochloride Basic information Product Name: 3,4-dihydroxy-α-aminoacetophenone hydrochloride Synonyms: 3,4-dihydroxy-α-aminoacetophenone hydrochloride;2-AMINO-1-(3,4-DIHYDROXYPHENYL)ETHANONE

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