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CAS No.: | 5090-29-9 |
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Name: | 3,4-dihydroxy-α-aminoacetophenone hydrochloride |
Molecular Structure: | |
Formula: | C8H9NO3 |
Molecular Weight: | 203.625 |
Synonyms: | Noradenalone hydrochloride;Noradrenalone Hydrochloride; |
Density: | 1.375g/cm3 |
Melting Point: | 255 °C |
Boiling Point: | 435.1°Cat760mmHg |
Flash Point: | 217°C |
PSA: | 83.55000 |
LogP: | 1.74150 |
1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid
norepinephrine hydrochloride
Conditions | Yield |
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With palladium 10% on activated carbon; hydrogen In methanol at 45℃; under 0.30003 - 0.375038 Torr; for 5h; Temperature; Pressure; Time; | 96.7% |
1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid
S-(-)-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeure-di-N,N'-1-(3,4-dihydroxyphenyl)-1-oxo-2-amido-ethan
Conditions | Yield |
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With sodium hydrogencarbonate In water; benzene for 30h; | 64.3% |
1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid
R-(+)-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeure-di-N,N'-1-(3,4-dihydroxyphenyl)-1-oxo-2-amido-ethan
Conditions | Yield |
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With sodium hydrogencarbonate In water; benzene for 30h; | 61.4% |
R,S-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeuredichlorid
1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid
R,S-2,2'-dinitrobiphenyl-6,6'-dicarbonsaeure-di-N,N'-1-(3,4-dihydroxyphenyl)-1-oxo-2-amido-ethan
Conditions | Yield |
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With sodium hydrogencarbonate In water; benzene for 30h; | 58.5% |
1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid
A
noradrenalone-3-O-sulfate
B
noradrenalone-4-O-sulfate
Conditions | Yield |
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With chlorosulfonic acid at -45 - -2℃; for 1h; Yield given; |
1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid
dl-norepinephrine-3-O-sulfate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chlorosulfonic acid / 1 h / -45 - -2 °C 2: NaBH4 / methanol; propan-2-ol / 7 h View Scheme |
1-(3,4-dihydroxyphenyl)-1-oxo-2-amino-ethan-hydrochlorid
dl-norepinephrine-4-O-sulfate
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: chlorosulfonic acid / 1 h / -45 - -2 °C 2: NaBH4 / methanol; propan-2-ol / 7 h View Scheme |
Conditions | Yield |
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Multi-step reaction with 3 steps 1: 58.5 percent / NaHCO3 / benzene; H2O / 30 h 2: 74 percent / NaBH4 / methanol / 24 h 3: 51.4 percent / H2, conc HCl / Pd/C / ethanol / 6 h / Ambient temperature View Scheme |
Conditions | Yield |
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Multi-step reaction with 3 steps 1: 61.4 percent / NaHCO3 / benzene; H2O / 30 h 2: NaBH4 / methanol / 24 h 3: 51.4 percent / H2, conc HCl / Pd/C / ethanol / 6 h / Ambient temperature View Scheme |
Conditions | Yield |
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Multi-step reaction with 3 steps 1: 64.3 percent / NaHCO3 / benzene; H2O / 30 h 2: NaBH4 / methanol / 24 h 3: 54.2 percent / H2, conc HCl / Pd/C / ethanol / 6 h / Ambient temperature View Scheme |