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CAS No.: | 52599-24-3 |
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Name: | N-T-BUTYL-N'-ISOPROPYLTHIOUREA |
Article Data: | 8 |
Molecular Structure: | |
Formula: | C8H18N2S |
Molecular Weight: | 174.31 |
Synonyms: | N-T-BUTYL-N'-ISOPROPYLTHIOUREA;1-Isopropyl-3-Tert-Butylthiourea |
Density: | 0.949±0.06 g/cm3(Predicted) |
Melting Point: | 150-152℃ |
Boiling Point: | 215.3±23.0 °C(Predicted) |
PSA: | 56.15000 |
LogP: | 2.43920 |
Conditions | Yield |
---|---|
In dichloromethane | 52% |
In dichloromethane | 52% |
Conditions | Yield |
---|---|
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h; | 52% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h; | 52% |
With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 2h; | 52% |
In chlorobenzene at 10 - 30℃; for 1h; Green chemistry; |
carbon disulfide
N,N,N′,N′-tetramethyl-N″-tert-butylguanidine
isopropylamine
A
1,1,3,3-tetramethyl-2-thiourea
B
N-tert-butyl-N'-isopropylthiourea
Conditions | Yield |
---|---|
1.) 0.5 h, 2.) room temperature, 1.5 h; Yield given. Multistep reaction. Yields of byproduct given; |
N-tert-butyl-N'-isopropylthiourea
N-Chloromethyl-N-phenylcarbamoyl chloride
buprofezin
Conditions | Yield |
---|---|
Stage #1: N-Chloromethyl-N-phenylcarbamoyl chloride With dipotassium peroxodisulfate; 3,6-dimethyl-3,6-dihydroperoxy-4,5-dioxaoctane at 40 - 45℃; Flow reactor; Large scale; Stage #2: N-tert-butyl-N'-isopropylthiourea With tetradecyltrimethylammonium chloride; calcium hydroxide at 15 - 50℃; Reagent/catalyst; Temperature; Flow reactor; Large scale; | 92.3% |
With sodium acetate In water; toluene at 30 - 45℃; for 2h; Temperature; Reagent/catalyst; | 87% |
With sodium hydrogencarbonate In water; chlorobenzene at 0 - 30℃; for 5.5h; Green chemistry; | |
With ammonia In 1,4-dioxane at 10 - 40℃; for 5h; Reagent/catalyst; |
N-tert-butyl-N'-isopropylthiourea
1-isopropylthiourea
Conditions | Yield |
---|---|
With hydrogenchloride In water for 0.666667h; Heating / reflux; | 90% |
In hydrogenchloride | 90% |
In hydrogenchloride | 90% |
With hydrogenchloride In water for 0.666667h; Heating / reflux; | 90% |
Stage #1: N-tert-butyl-N'-isopropylthiourea With hydrogenchloride; water for 0.666667h; Heating / reflux; Stage #2: With water; sodium hydrogencarbonate at 0℃; pH=9.5; Saturated solution; | 90% |
N-tert-butyl-N'-isopropylthiourea
Conditions | Yield |
---|---|
With potassium hydroxide In benzene | 62% |
1,3,5-tris(o-isopropyl)phenyl-hexahydro-s-triazine
N-tert-butyl-N'-isopropylthiourea
trichloromethyl chloroformate
2-tert-butylimino-3-isopropyl-5-(2-isopropyl-phenyl)-[1,3,5]thiadiazinan-4-one
Conditions | Yield |
---|---|
With potassium hydroxide In tetrahydrofuran; benzene | 52% |
N-tert-butyl-N'-isopropylthiourea
N,N′-diisopropylcarbodiimide
Conditions | Yield |
---|---|
With lead dioxide In water Heating; | 50% |
N-tert-butyl-N'-isopropylthiourea
1,3,5-tris(p-tolyl)hexahydro-s-triazine
trichloromethyl chloroformate
Conditions | Yield |
---|---|
With sodium hydroxide In tetrahydrofuran; benzene | 45% |
N-tert-butyl-N'-isopropylthiourea
trichloromethyl chloroformate
Conditions | Yield |
---|---|
With sodium hydroxide | 45% |