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| CAS No.: | 53185-12-9 |
|---|---|
| Name: | fagomine |
| Article Data: | 24 |
| Molecular Structure: | |
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| Formula: | C6H13 N O3 |
| Molecular Weight: | 147.174 |
| Synonyms: | 3,4-Piperidinediol,2-(hydroxymethyl)-, [2R-(2a,3b,4a)]-; 1,2,5-Trideoxy-1,5-imino-D-arabino-hexitol;D-Fagomine; Fagomine |
| Density: | 1.279g/cm3 |
| Melting Point: | 185-186℃ |
| Boiling Point: | 315.4°Cat760mmHg |
| Flash Point: | 170.5°C |
| PSA: | 72.72000 |
| LogP: | -1.60880 |
- 81281-59-67-Benzylideneaminotheophylline
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- 73441-42-6METHYL-5-CHLORO-2,2-DIMETHYLVALERATE
- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 958254-66-51H-Imidazo[4,5-b]pyridine-2-carboxaldehyde, 1-methyl-, hydrochloride
- 99170-93-1N-Methyl-2-oxazolamine
- 717878-06-31-(4-fluorophenyl)-4-nitro-1H-imidazole
- 914458-26-7[5-(2-fluorophenyl)-1-pentyl-1H-pyrrol-3-yl]-1-naphthalenyl-Methanone
- 548773-13-32-amino-4,6-dimethylpyrimidine-5-carboxylic acid
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| With triethylsilane; palladium on activated charcoal; hydrogen In ethanol at 20℃; | 100% |
- 1430587-89-5
(2R,3R,4R)-benzyl 3,4-bis(benzyloxy)-2-(hydroxymethyl)piperidine-1-carboxylate
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| With hydrogenchloride; palladium on activated charcoal; hydrogen In ethanol; water for 12h; Inert atmosphere; | 95% |
- 366815-76-1
(2R,3R,4R)-3,4-bis(benzyloxy)-2-((benzyloxy)methyl)piperidine
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| With palladium 10% on activated carbon; hydrogen; acetic acid at 27℃; for 12h; | 87% |
| With hydrogenchloride; palladium 10% on activated carbon; hydrogen In methanol at 20℃; under 2585.81 Torr; for 18h; | 82% |
- 768387-41-3
(4aR,8R,8aR)-tert-butyl hexahydro-8-hydroxy-2,2-dimethyl[1,3]dioxino[5,4-b]pyridine-5-carboxylate
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| Stage #1: (4aR,8R,8aR)-tert-butyl hexahydro-8-hydroxy-2,2-dimethyl[1,3]dioxino[5,4-b]pyridine-5-carboxylate With hydrogenchloride In methanol; water at 60℃; for 2h; Stage #2: With DOWEX-50wX8 Further stages.; | 83% |
| With hydrogenchloride In methanol; ethyl acetate for 2h; |
- 121742-14-1
(3S,4R)-6-[(benzyloxycarbonyl)amino]-5,6-dideoxy-2-hexulose
A
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| With hydrogen; palladium on activated charcoal In ethanol; water at 20℃; under 2585.81 Torr; | A 83% B n/a |
- 354153-41-6
(1S,2R,6R)-2-(tert-butyldiphenylsilanyloxymethyl)-7-oxa-3-azabicyclo[4.1.0]heptane-3-carboxylic acid tert-butyl ester
A
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| Stage #1: (1S,2R,6R)-2-(tert-butyldiphenylsilanyloxymethyl)-7-oxa-3-azabicyclo[4.1.0]heptane-3-carboxylic acid tert-butyl ester With potassium hydroxide In 1,4-dioxane Stage #2: With hydrogenchloride In methanol at 60℃; for 1h; | A 17% B 82% |
| With sulfuric acid In 1,4-dioxane; water | A 44% B 33% |
| With sulfuric acid In 1,4-dioxane; water at 95℃; for 3h; | A 44% B 33% |
- 1349697-04-6
(2R,3R,4R)-3-(tert-butyldimethylsilyloxy)-2-((tert-butyldimethylsilyloxy)methyl)piperidin-4-ol
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| With hydrogenchloride; water at 20℃; for 24h; | 82% |
- 115827-05-9
5,6-dideoxy-6(trifluoroacetamido)-D-threo-hexulose
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| With 10 wt% Pd(OH)2 on carbon; hydrogen; potassium carbonate In water under 2585.81 Torr; | 81% |
- 1129725-82-1
(2S,3R,4R)-1-benzyl-3,4-bis(benzyloxy)-2-[(benzyloxy)methyl]piperidine
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| With palladium 10% on activated carbon; hydrogen In methanol at 20℃; under 2585.81 Torr; for 24h; | 80% |
- 354153-40-5
(1R,2R,6S)-2-(tert-butyldiphenylsilanyloxymethyl)-7-oxa-3-azabicyclo[4.1.0]heptane-3-carboxylic acid tert-butyl ester
- 53185-12-9
D-fagomine
| Conditions | Yield |
|---|---|
| With sulfuric acid In 1,4-dioxane; water | 75% |
| With sulfuric acid In 1,4-dioxane; water at 95℃; for 3h; | 75% |
- Total:35 Page 1 of 1 1
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