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CAS No.: | 53185-52-7 |
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Name: | 3-methoxy-N,N-dimethylpropionamide |
Article Data: | 9 |
Molecular Structure: | |
Formula: | C6H13 N O2 |
Molecular Weight: | 131.175 |
Synonyms: | N,N-Dimethyl-3-methoxypropionamide |
Density: | 0.948g/cm3 |
Boiling Point: | 188.7°Cat760mmHg |
Flash Point: | 67.9°C |
Solubility: | 500g/L at 21.5℃ |
PSA: | 29.54000 |
LogP: | 0.11110 |
methyl 3-methoxypropionate
dimethyl amine
β-methoxy-N,N-dimethylpropionic acid amide
Conditions | Yield |
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With zinc(II) trifluoroacetate at 0 - 40℃; for 8h; Reagent/catalyst; Autoclave; | 99% |
With sodium methylate; glycerol at 60℃; for 6h; Autoclave; | 86% |
With potassium tert-butylate at 20℃; under 600.06 Torr; for 4h; Product distribution / selectivity; Autoclave; | |
With sodium methylate; ethylene glycol at 60℃; for 8h; Product distribution / selectivity; Autoclave; |
Conditions | Yield |
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at 60℃; for 6h; Autoclave; |
Conditions | Yield |
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With sodium methylate at 20 - 40℃; Product distribution / selectivity; Inert atmosphere; | |
With 2-Cyanopyridine; cerium(IV) oxide at 49.84℃; for 24h; Kinetics; |
3-(N,N-dimethylamino)-N',N'-dimethylpropionamide
β-methoxy-N,N-dimethylpropionic acid amide
Conditions | Yield |
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Multi-step reaction with 2 steps 1: hydroquinone; cupferron / alumina N611N / water / 5 h / 250 °C / 2250.23 Torr 2: sodium methylate / 20 - 40 °C / Inert atmosphere View Scheme |
3-Methoxypropionic acid
dimethyl amine
β-methoxy-N,N-dimethylpropionic acid amide
Conditions | Yield |
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at 100℃; under 11251.1 Torr; Temperature; Pressure; | |
at 100℃; under 11251.1 Torr; Temperature; Pressure; Concentration; |
β-methoxy-N,N-dimethylpropionic acid amide
N,N-Dimethylacrylamide
Conditions | Yield |
---|---|
With 4-methoxy-phenol; potassium hydroxide In ethylene glycol at 200℃; Temperature; Reagent/catalyst; Pyrolysis; | 98% |
With 10H-phenothiazine; copper(II) bis(trifluoromethanesulfonate) at 130℃; for 6h; Inert atmosphere; | 92% |
β-methoxy-N,N-dimethylpropionic acid amide
4-chlorobenzoic acid hydrazide
Conditions | Yield |
---|---|
With titanium tetrachloride at 110℃; for 1.5h; | 74% |