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CAS No.: | 5687-07-0 |
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Name: | 1,5-DIAZACYCLOOCTANE |
Article Data: | 15 |
Molecular Structure: | |
Formula: | C6H14 N2 |
Molecular Weight: | 114.191 |
Synonyms: | (1,5)Diazocane;1,5-Diazacyclooctane; Octahydro-1,5-diazocine |
Density: | 0.852 |
Boiling Point: | 194ºC |
Flash Point: | 84ºC |
PSA: | 24.06000 |
LogP: | 0.61700 |
1,5-diazabicyclooctane dihydrobromide
1,5-diazacyclooctane
Conditions | Yield |
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With sodium methylate In methanol at 70℃; for 0.166667h; | 98% |
1,5-bis(p-toluenesulphonyl)-1,5-diazacyclooctane
1,5-diazacyclooctane
Conditions | Yield |
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With hydrogen bromide; phenol at 80℃; for 60h; | 86% |
Conditions | Yield |
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at 120℃; im Rohr; |
Conditions | Yield |
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With water; nickel Hydrogenation; | |
With diisobutylaluminum hydride |
N1-(cyanoethyl)-1,3-propanediamine
1,5-diazacyclooctane
Conditions | Yield |
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With sodium; butan-1-ol |
Conditions | Yield |
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With tetrafluoroboric acid for 0.5h; Product distribution; Heating; t1/2; further reagent:NaOH/D2O; |
1,5-diazacyclooctane
Conditions | Yield |
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With hydrogenchloride at 180℃; |
ethanol
1,3-Dichloropropane
hydrazine
A
pyrazolidine
B
1,5-diazacyclooctane
3-propyl tosylate
1,5-diazacyclooctane
Conditions | Yield |
---|---|
Multi-step reaction with 2 steps 1: 1.) sodium hydride / 1.) DMF, 80 deg C, 2.5 h, 2.) DMF, 80 deg C, 24 h 2: 86 percent / phenol, 33percent HBr in acetic acid / 60 h / 80 °C View Scheme |
N-tosyl-bis(3-hydroxypropyl)amine
1,5-diazacyclooctane
Conditions | Yield |
---|---|
Multi-step reaction with 3 steps 1: 65 percent / triethylamine, 4-dimethylaminopyridine (DMAP) / CH2Cl2 / 2 h / Ambient temperature 2: 1.) sodium hydride / 1.) DMF, 80 deg C, 2.5 h, 2.) DMF, 80 deg C, 24 h 3: 86 percent / phenol, 33percent HBr in acetic acid / 60 h / 80 °C View Scheme |