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Basic Information
CAS No.: 57280-22-5
Name: 4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane
Article Data: 12
Molecular Structure:
Molecular Structure of 57280-22-5 (4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane)
Formula: C7H12O3
Molecular Weight: 144.17
Synonyms: 4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane
Density: 1.071
Boiling Point: 179℃
Flash Point: 56℃
Hazard Symbols:
Risk Codes: 36-43
Safety:
Hazard Codes Xi
Risk Statements 36-43
Safety Statements 26-36/37
PSA: 30.99000
LogP: 0.53670
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Conditions
ConditionsYield
With disodium hydrogenphosphate; dihydrogen peroxide; sodium hydroxide In methanol; water; acetonitrile at 60 - 80℃; pH=7 - 9.5; Large scale; Green chemistry;85.2%
With disodium hydrogenphosphate; 3-chloro-benzenecarboperoxoic acid In dichloromethane at 20℃; for 18h; Inert atmosphere;85%
With disodium hydrogenphosphate; dihydrogen peroxide; Hexafluoroacetone In 1,2-dichloro-ethane for 24h; Heating;83%
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4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1: toluene-4-sulfonic acid / dichloromethane / 3 h / 20 °C / Inert atmosphere
2: 3-chloro-benzenecarboperoxoic acid; disodium hydrogenphosphate / dichloromethane / 18 h / 20 °C / Inert atmosphere
View Scheme

C7H13BrO3

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4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane

Conditions
ConditionsYield
With potassium carbonate In methanol at 20℃; for 16h;19 g
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Conditions
ConditionsYield
In ethanol epoxide:amine=2:1;100%
57280-22-5

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benzylamine

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trans-6-benzylamino-2,2'-dimethyl-1,3-dioxocycloheptan-5-ol

Conditions
ConditionsYield
Stage #1: benzylamine With titanium(IV) isopropylate; (R)-1,1'-Bi-2-naphthol; (R)-6,6'-dibromo-1,1'-binaphth-2-ol In toluene at 20℃; for 0.5h;
Stage #2: 4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane With water In toluene at 40℃; for 12h; optical yield given as %ee;		99%
With titanium(IV) isopropylate; (R)-1,1'-Bi-2-naphthol In toluene enantioselective reaction;78%
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4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane

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benzylamine

(5R,6S)-6-(benzylamino)-2,2-dimethyl-1,3-dioxepan-5-ol

Conditions
ConditionsYield
With C92H72N2O6*2Ti*2O In water; toluene at 40℃; for 18h; Reagent/catalyst; Inert atmosphere; Green chemistry;99%
Stage #1: benzylamine With titanium(IV) isopropylate; C20H24O2; (R)-3,3'-diiodo-2,2'-dihydroxy-1,1'-binaphthyl In toluene at 20℃; for 0.5h;
Stage #2: 4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane With water In toluene at 40℃; for 12h; optical yield given as %ee;		27%
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Conditions
ConditionsYield
With potassium carbonate In isopropyl alcohol at 60℃; for 12h; Reagent/catalyst; Temperature;99%
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Conditions
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In ethanol epoxide:amine=1:1; addition of epoxide to amine dropwise over 1 h;98%
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thiophenol

(2R*,3R*)-1,4-di-O-isopropylidene-3-phenylthio-1,2,4-butanetriol

Conditions
ConditionsYield
With sodium hydride In tetrahydrofuran 0 deg C, 30 min, reflux, 1 h;96.9%
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bis(3-aminopropyl)amine

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4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]-octane

6-[3-(3-Amino-propylamino)-propylamino]-2,2-dimethyl-[1,3]dioxepan-5-ol

Conditions
ConditionsYield
In ethanol epoxide:amine=1:1; addition of epoxide to amine dropwise over 1 h;92%
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  • 4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]octane

  • Casno:

    57280-22-5

    4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]octane

    Min.Order: 4 Kilogram

    FOB Price:  USD $ 0.0-0.0

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  • 4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

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    57280-22-5

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  • 3,5,8-Trioxabicyclo[5.1.0]octane, 4,4-diMethyl- CAS NO.57280-22-5

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    57280-22-5

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  • 4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

  • Casno:

    57280-22-5

    4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

    Min.Order: 1 Kilogram

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  • Casno:

    57280-22-5

    4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

    Min.Order: 1 Gram

    FOB Price:  USD $ 0.0-0.0

    Product Name: 4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane Synonyms: 4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane;3,5,8-Trioxabicyclo[5.1.0]octane, 4,4-diMethyl-;4,4-diMethyl-3,5,8-trioxabicyclo[5.1.0]octane(EP2);4,4-Dimethyl-3,5,8-trioxabi

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  • 4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

  • Casno:

    57280-22-5

    4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

    Min.Order: 1 Kilogram

    FOB Price:  USD $ 18.0-20.0

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  • Casno:

    57280-22-5

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    Product name: 4,4-Dimethyl-3,5,8-Trioxabicyclo[5.1.0]octane CAS No.: 57280-22-5 Molecule Formula：C7H12O3 Molecule Weight：144.17 Purity: 99.0% Package: 25kg/drum Description：White or off-white powder Manufacture Standards：Enterprise St

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    57280-22-5

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  • Casno:

    57280-22-5

    4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

    Min.Order: 1 Gram

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  • 4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

  • Casno:

    57280-22-5

    4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

    Min.Order: 1 Metric Ton

    FOB Price:  USD $ 1.5-1.5

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  • SAGECHEM/ 4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]octane /Manufacturer in China

  • Casno:

    57280-22-5

    SAGECHEM/ 4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]octane /Manufacturer in China

    Min.Order: 0 Metric Ton

    FOB Price:  USD $ 0.0-0.0

    SAGECHEM is a chemical R&D, manufacturing and distribution company in China since 2009, including pharmaceutical intermediates, agrochemical, dyestuff intermediates, organosilicone, API and etc. We also offer a full range of services in

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  • Casno:

    57280-22-5

    4,4-Dimethyl-3,5,8-trioxabicyclo[5.1.0]octane

    Min.Order: 0

    FOB Price:  USD $ 0.0-0.0

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  • Casno:

    57280-22-5

    4,4-Dimethyl-3,5,8-trioxabic-yclo[5,1,0]Octane

    Min.Order: 1 Metric Ton

    FOB Price:  USD $ 1.0-1.0

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  • 4,4-Dimethyl-3,5,8-trioxabicyclo[5.1.0]octane cas no. 57280-22-5 98%

  • Casno:

    57280-22-5

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  • Casno:

    57280-22-5

    4,4-dimethyl-3,5,8-trioxabicyclo[5.1.0]octane

    Min.Order: 0

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    57280-22-5

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    Min.Order: 0

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     China (Mainland)  |  Contact Details

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