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| CAS No.: | 5821-51-2 |
|---|---|
| Name: | Corannulene |
| Article Data: | 29 |
| Molecular Structure: | |
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| Formula: | C20H10 |
| Molecular Weight: | 250.299 |
| Synonyms: | corranulene;Dibenzo[ghi,mno]fluoranthene;[5]circulene;Coarannulen; |
| Density: | 1.467g/cm3 |
| Melting Point: | 269°C(lit.) |
| Boiling Point: | 437.997°C at 760 mmHg |
| Flash Point: | 210.065°C |
| PSA: | 0.00000 |
| LogP: | 5.76600 |
- 81281-59-67-Benzylideneaminotheophylline
- 82993-81-5D-threo-Ritalinic acid hydrochloride
- 73441-42-6METHYL-5-CHLORO-2,2-DIMETHYLVALERATE
- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 958254-66-51H-Imidazo[4,5-b]pyridine-2-carboxaldehyde, 1-methyl-, hydrochloride
- 99170-93-1N-Methyl-2-oxazolamine
- 717878-06-31-(4-fluorophenyl)-4-nitro-1H-imidazole
- 914458-26-7[5-(2-fluorophenyl)-1-pentyl-1H-pyrrol-3-yl]-1-naphthalenyl-Methanone
- 894852-01-87-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
- 289721-44-4
1,2,5,6-tetrabromocorannulene
- 5821-51-2
Coarannulen
| Conditions | Yield |
|---|---|
| With hydrogenchloride; potassium iodide; zinc In ethanol for 6h; Heating; | 91% |
| With potassium iodide; zinc In ethanol for 6h; Heating; | 90% |
| With potassium iodide; zinc In N,N-dimethyl-formamide at 160℃; for 24 - 36h; | 70% |
- 138982-82-8
1,6,7,10-tetrakis(bromomethyl)fluoranthene
- 5821-51-2
Coarannulen
| Conditions | Yield |
|---|---|
| With titanium tetrachloride; copper; zinc In 1,2-dimethoxyethane for 48h; | 80% |
| at 1000℃; | 18% |
| Multi-step reaction with 3 steps 1: 75 percent / Na2S / acetone 2: 70 percent / H2O2, acetic acid 3: 400 °C View Scheme |
- 244236-72-4
1,6,7,10-tetrakis(dibromomethyl)fluoranthene
- 5821-51-2
Coarannulen
| Conditions | Yield |
|---|---|
| With titanium tetrachloride; copper; zinc In 1,2-dimethoxyethane for 120h; Cyclization; Heating; | 80% |
| With lithium aluminium tetrahydride; vanadium(III) chloride In 1,2-dimethoxyethane for 8h; Cyclization; Heating; | 73% |
| Stage #1: 1,6,7,10-tetrakis(dibromomethyl)fluoranthene With sodium hydroxide In water; acetone for 1h; Reflux; Stage #2: With n-butyllithium In tetrahydrofuran at -78℃; for 0.5h; | 55% |
- 243853-48-7
1,3,5,7,9-pentachlorocorannulene
- 5821-51-2
Coarannulen
| Conditions | Yield |
|---|---|
| With copper(l) iodide; 1,10-Phenanthroline; caesium carbonate; tert-butyl alcohol In N,N-dimethyl-formamide at 220℃; for 2h; Microwave irradiation; | 71% |
- 135584-70-2
7,10-Bis-(2,2-dibromo-vinyl)-fluoranthene
- 5821-51-2
Coarannulen
| Conditions | Yield |
|---|---|
| at 1000℃; | 40% |
| at 1000℃; under 0.6 Torr; | 21% |
| Multi-step reaction with 2 steps 1: 80 percent / LDA / tetrahydrofuran / 5 h / -78 °C 2: 10 percent / 18 h / 1000 °C / 0.6 Torr View Scheme | |
| Multi-step reaction with 2 steps 1: 80 percent / lithium diisopropylamide / tetrahydrofuran / 5 h / -78 °C 2: 10 percent / 1000 °C View Scheme |
- 5821-51-2
Coarannulen
| Conditions | Yield |
|---|---|
| at 1100℃; under 1 Torr; for 24h; | 39% |
| at 1100℃; | 11.4% |
- 253801-43-3
7,10-bis(trimethylsilylethynyl)fluoroanthrene
- 5821-51-2
Coarannulen
| Conditions | Yield |
|---|---|
| at 1000℃; under 0.900072 Torr; Cyclization; flash vacuum pyrolysis; | 36% |
- 135584-70-2
7,10-Bis-(2,2-dibromo-vinyl)-fluoranthene
A
- 5821-51-2
Coarannulen
B
- 138816-09-8
monobromocorannulene
C
- 138816-10-1
1,6-dibromocorannulene
| Conditions | Yield |
|---|---|
| at 900℃; | A 23% B 29% C 2.4% |
| at 900℃; under 0.6 Torr; for 24h; | A 23% B 29% C 2.4% |
- 157729-37-8
3-(4H-cyclopentaphenanthrylidene)-1,5-bis(trimethylsilyl)-1,4-pentadiyne
A
- 129-00-0
pyrene
B
- 192-97-2
benzo[e]pyrene
C
- 203-64-5
4H-Cyclopenta[def]phenanthrene
D
- 27208-37-3
cyclopenta[c,d]pyrene
E
- 203-12-3
benzo[ghi]fluoranthene
F
- 5821-51-2
Coarannulen
| Conditions | Yield |
|---|---|
| With hydrogen In gas at 900℃; Product distribution; electrically heated vertical laboratory tubular furnace; | A n/a B n/a C n/a D n/a E n/a F 15% |
- 157729-37-8
3-(4H-cyclopentaphenanthrylidene)-1,5-bis(trimethylsilyl)-1,4-pentadiyne
A
- 129-00-0
pyrene
B
- 192-97-2
benzo[e]pyrene
C
- 27208-37-3
cyclopenta[c,d]pyrene
D
- 5821-51-2
Coarannulen
| Conditions | Yield |
|---|---|
| With hydrogen In gas at 900℃; electrically heated vertical laboratory tubular furnace; Further byproducts given; | A n/a B n/a C n/a D 15% |
- Total:18 Page 1 of 1 1
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