Name: 2,5-Dimethoxy-4-nitroaniline
SKU: 6313-37-7

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Basic Information

Molecular Structure:
CAS No.:	6313-37-7
Name:	2,5-Dimethoxy-4-nitroaniline
Article Data:	9

Formula:	C₈H₁₀N₂O₄
Molecular Weight:	198.178
Synonyms:	Aniline,2,5-dimethoxy-4-nitro- (6CI,8CI);1-Amino-2,5-dimethoxy-4-nitrobenzene;2,5-Dimethoxy-4-nitroaniline;3,6-Dimethoxy-4-nitroaniline;NSC 39868;
EINECS:	228-640-8
Density:	1.307 g/cm³
Melting Point:	152-155 °C(lit.)
Boiling Point:	401.5 °C at 760 mmHg
Flash Point:	196.6 °C
Appearance:	dark khaki granular crystalline powder
Hazard Symbols:	Xn
Risk Codes:	20/21/22
Safety:	36/37
Transport Information:	UN 2811 6.1/PG 3
PSA:	90.30000
LogP:	2.29860

Synthetic route

: 262436-38-4
N-(2,5-dimethoxy-4-nitrophenyl)thiobenzamide

: 6313-37-7
2,5-dimethoxy-4-nitroaniline

Conditions

Conditions	Yield
With hydrogen carbonate In methanol for 24h; Deacylation; Heating;	100%

: 89-39-4
1,4-dimethoxy-2-nitrobenzene

A: 6313-37-7
2,5-dimethoxy-4-nitroaniline

B: 26002-57-3
2-amino-3-nitrohydroquinone dimethylether

Conditions

Conditions	Yield
Stage #1: 1,4-dimethoxy-2-nitrobenzene With pyridine; trifluorormethanesulfonic acid; lithium perchlorate In acetonitrile at 25℃; Electrochemical reaction; Stage #2: With piperidine In acetonitrile at 80℃; for 12h; Electrochemical reaction; Overall yield = 95 %;	A 66% B 30%

: 110-86-1
pyridine

: 89-39-4
1,4-dimethoxy-2-nitrobenzene

A: 6313-37-7
2,5-dimethoxy-4-nitroaniline

B: 26002-57-3
2-amino-3-nitrohydroquinone dimethylether

Conditions

Conditions	Yield
Stage #1: pyridine; 1,4-dimethoxy-2-nitrobenzene With ammonium peroxydisulfate; tris(1,10-phenathrolinyl)ruthenium(II) hexafluorophosphate In water; acetonitrile at 23℃; for 24h; Irradiation; Inert atmosphere; Schlenk technique; Stage #2: With pyrrolidine at 70℃; for 12h;	A 13% B 41 mg

...Expand

: 25445-13-0
2,5-dimethoxy-4-nitroacetanilide

: 6313-37-7
2,5-dimethoxy-4-nitroaniline

Conditions

Conditions	Yield
durch Verseifen;
With hydrogenchloride

: 108851-78-1
N,N'-bis-(2,5-dimethoxy-4-nitro-phenyl)-urea

: 6313-37-7
2,5-dimethoxy-4-nitroaniline

Conditions

Conditions	Yield
With ammonium hydroxide at 150℃;

4-chloro-5-nitro-2-amino-phenol-methyl ether: 4-chloro-5-nitro-2-amino-phenol-methyl ether

: 6313-37-7
2,5-dimethoxy-4-nitroaniline

Conditions

Conditions	Yield
With potassium carbonate

: C18H26N2O8

: 6313-37-7
2,5-dimethoxy-4-nitroaniline

Conditions

Conditions	Yield
With potassium carbonate In methanol Heating;

: 135-45-5
N-(2,5-Dimethoxyphenyl)benzamide

: 6313-37-7
2,5-dimethoxy-4-nitroaniline

Conditions

Conditions	Yield
Multi-step reaction with 3 steps 1: 89 percent / HNO3; H2O / acetic acid / 1.5 h / 20 °C 2: 79 percent / Lawesson's reagent / toluene / 12 h / 80 °C 3: 100 percent / HCO3(-) / methanol / 24 h / Heating View Scheme

: 92-20-6
N-(2,5-Dimethoxy-4-nitrophenyl)benzamide

: 6313-37-7
2,5-dimethoxy-4-nitroaniline

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: 79 percent / Lawesson's reagent / toluene / 12 h / 80 °C 2: 100 percent / HCO3(-) / methanol / 24 h / Heating View Scheme

: 1240-72-8
1,3-bis(2,5-dimethoxyphenyl)urea

: 6313-37-7
2,5-dimethoxy-4-nitroaniline

Conditions

Conditions	Yield
Multi-step reaction with 2 steps 1: aqueous nitric acid <86 percent >; acetic acid 2: aqueous ammonia / 150 °C View Scheme

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Chemistry

The molecular formula of 2,5-Dimethoxy-4-nitroaniline(6313-37-7) is C₈H₁₀N₂O₄ and its formula weight is 198.18.
2,5-Dimethoxy-4-nitroaniline(6313-37-7) has a melting point of 152-155 °C(lit.).
The chemical synonyms of 2,5-Dimethoxy-4-nitroaniline (6313-37-7) are TIMTEC-BB SBB000371;2,5-DIMETHOXY-4-NITROANILINE;2,5-DIMETHOXY-4-NITROBENZENAMINE;2,5-dimethoxy-4-nitro-benzenamin;2,5-DIMETHOXY-4-NITROANILINE, 98+%;Benzenamine, 2,5-dimethoxy-4-nitro-
The molecular structure of 2,5-Dimethoxy-4-nitroaniline(6313-37-7):

Toxicity Data With Reference

RTECS#: CAS# 6313-37-7: None listed
LD50/LC50: RTECS: Not available.
Carcinogenicity: 2,5-Dimethoxy-4-nitroaniline - Not listed as a carcinogen by ACGIH, IARC, NTP, or CA Prop 65.
Other: The toxicological properties have not been fully investigated.

Safety Profile

Hazard Codes Xn
Risk Statements 20/21/22
Safety Statements 36-36/37
RIDADR UN 2811 6.1/PG 3
WGK Germany 3

Specification

Chemical Stability: Stable under normal temperatures and pressures.
Conditions to Avoid: Incompatible materials.
Incompatibilities with Other Materials Strong oxidizing agents, acids, strong bases, acid chlorides, acid anhydrides, chloroformates.
Hazardous Decomposition Products Nitrogen oxides, carbon monoxide, carbon dioxide.
Hazardous Polymerization Has not been reported.