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63486-45-3

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Basic Information
CAS No.: 63486-45-3
Name: 1,3-Cyclopentanediamine,cis-(9CI)
Article Data: 4
Molecular Structure:
Molecular Structure of 63486-45-3 (1,3-Cyclopentanediamine,cis-(9CI))
Formula: C5H12N2
Molecular Weight: 100.164
Synonyms: 1,3-Cyclopentanediamine,cis-(9CI)
Density: 0.964±0.06 g/cm3(Predicted)
Boiling Point: 172.7±8.0 °C(Predicted)
PSA: 52.04000
LogP: 1.22550
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63486-45-3

(1R,3S)-cyclopentane-1,3-diamine

Conditions
ConditionsYield
With palladium 10% on activated carbon; hydrogen In methanol at 30℃; for 16h;93%
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di-tert-butyl dicarbonate

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(1R,3S)-cyclopentane-1,3-diamine

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3,6-diiodopyridazine

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Conditions
ConditionsYield
Stage #1: (1R,3S)-cyclopentane-1,3-diamine; 3,6-diiodopyridazine With potassium phosphate; copper(l) iodide; N,N-dimethyl-formamide; ethylene glycol for 12h; Heating;
Stage #2: di-tert-butyl dicarbonate In ethylene glycol; ethyl acetate at 25℃; for 1h;		74%
...Expand
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methyl 1-(2,2-dihydroxyethyl)-4-oxo-3-[(phenylmethyl)oxy]-1,4-dihydro-2-pyridinecarboxylate

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(1R,3S)-cyclopentane-1,3-diamine

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Conditions
ConditionsYield
With acetic acid In toluene at 90℃; for 1.5h;57%
63486-45-3

(1R,3S)-cyclopentane-1,3-diamine

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1,1'-carbonyldiimidazole

1-((1R,3S)-3-aminocyclopentyl)-3-(6-((R)-2-(2,5-difluorophenyl)pyrrolidin-1-yl)-[1,2,4]triazolo[4,3-a]pyrazin-3-yl)urea

Conditions
ConditionsYield
Stage #1: C15H14F2N6; 1,1'-carbonyldiimidazole With N-ethyl-N,N-diisopropylamine In toluene at 20℃; for 1h;
Stage #2: (1R,3S)-cyclopentane-1,3-diamine In toluene for 8h;		56.4%
...Expand
63486-45-3

(1R,3S)-cyclopentane-1,3-diamine

N,N'-bis-(3-amino-cyclopentyl)-pyridazine-3,6-diamine

Conditions
ConditionsYield
Multi-step reaction with 2 steps
1.1: CuI; K3PO4; DMF / ethylene glycol / 12 h / Heating
1.2: 74 percent / ethyl acetate; ethane-1,2-diol / 1 h / 25 °C
2.1: CF3CO2H / 0.5 h / 0 °C
View Scheme
63486-45-3

(1R,3S)-cyclopentane-1,3-diamine

N,N'-bis-[3-(tetrazolo[1,5-b]pyridazin-6-ylamino)-cyclopentyl]-pyridazine-3,6-diamine

Conditions
ConditionsYield
Multi-step reaction with 3 steps
1.1: CuI; K3PO4; DMF / ethylene glycol / 12 h / Heating
1.2: 74 percent / ethyl acetate; ethane-1,2-diol / 1 h / 25 °C
2.1: CF3CO2H / 0.5 h / 0 °C
3.1: 0.094 g / K2CO3 / dimethylformamide / 8 h / 95 °C
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63486-45-3

(1R,3S)-cyclopentane-1,3-diamine

C46H80N12P2

Conditions
ConditionsYield
Multi-step reaction with 4 steps
1.1: CuI; K3PO4; DMF / ethylene glycol / 12 h / Heating
1.2: 74 percent / ethyl acetate; ethane-1,2-diol / 1 h / 25 °C
2.1: CF3CO2H / 0.5 h / 0 °C
3.1: 0.094 g / K2CO3 / dimethylformamide / 8 h / 95 °C
4.1: 60 percent / acetonitrile / 3 h / Heating
View Scheme
63486-45-3

(1R,3S)-cyclopentane-1,3-diamine

C60H86N12O8

Conditions
ConditionsYield
Multi-step reaction with 5 steps
1.1: CuI; K3PO4; DMF / ethylene glycol / 12 h / Heating
1.2: 74 percent / ethyl acetate; ethane-1,2-diol / 1 h / 25 °C
2.1: CF3CO2H / 0.5 h / 0 °C
3.1: 0.094 g / K2CO3 / dimethylformamide / 8 h / 95 °C
4.1: 60 percent / acetonitrile / 3 h / Heating
5.1: toluene / 24 h / Heating
View Scheme
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4,7-dichloroquinoline

dimethanesulphonate

dimethanesulphonate

63486-45-3

(1R,3S)-cyclopentane-1,3-diamine

cis-N,N'-bis-(7-chloroquinolin-4-yl)-cyclopentane-1,3-diamine

Conditions
ConditionsYield
With methanesulfonic acid; triethylamine In diethyl ether; acetic acid
...Expand
63486-45-3

(1R,3S)-cyclopentane-1,3-diamine

C12H8ClN3O

C17H19N5O

Conditions
ConditionsYield
With triethylamine In ethanol at 120℃; for 1h;
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