Products Categories
Basic Information
| CAS No.: | 63648-81-7 |
|---|---|
| Name: | Sucrose-6-acetic ester |
| Article Data: | 19 |
| Molecular Structure: | |
|
|
|
| Formula: | C14H24 O12 |
| Molecular Weight: | 384.337 |
| Synonyms: | Sucrose6-acetate |
| Density: | 1.66±0.1 g/cm3(Predicted) |
| Melting Point: | 116 - 118°C |
| Boiling Point: | 674.6±55.0 °C(Predicted) |
| PSA: | 195.60000 |
| LogP: | -4.82480 |
Related products
- 81281-59-67-Benzylideneaminotheophylline
- 82993-81-5D-threo-Ritalinic acid hydrochloride
- 73441-42-6METHYL-5-CHLORO-2,2-DIMETHYLVALERATE
- 68439-39-4Poly(oxy-1,2-ethanediyl), alpha-(2-ethylhexyl)-omega-hydroxy-,
- 852475-26-4MC1568
- 958254-66-51H-Imidazo[4,5-b]pyridine-2-carboxaldehyde, 1-methyl-, hydrochloride
- 99170-93-1N-Methyl-2-oxazolamine
- 717878-06-31-(4-fluorophenyl)-4-nitro-1H-imidazole
- 914458-26-7[5-(2-fluorophenyl)-1-pentyl-1H-pyrrol-3-yl]-1-naphthalenyl-Methanone
- 894852-01-87-BROMO-2,2-DIMETHYL-2H-PYRIDO[3,2-B][1,4]OXAZIN-3(4H)-ONE
Synthetic route
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: Sucrose With di(n-butyl)tin oxide In cyclohexane; N,N-dimethyl-formamide at 60 - 95℃; for 5h; Stage #2: acetic anhydride In cyclohexane; N,N-dimethyl-formamide at 5 - 20℃; for 4.5h; | 98.6% |
| Stage #1: Sucrose With 1,3-diacetoxy-1,1,3,3-tetrabutyldistannoxane In cyclohexane; N,N-dimethyl-formamide for 0.08h; Heating / reflux; Azeotropic water co-distillation; Stage #2: acetic anhydride In cyclohexane; N,N-dimethyl-formamide at 10℃; for 2h; | |
| Stage #1: Sucrose; di(n-butyl)tin oxide In N,N-dimethyl-formamide at 80 - 85℃; for 10 - 13h; Stage #2: acetic anhydride In N,N-dimethyl-formamide at 0 - 20℃; for 3 - 4h; Product distribution / selectivity; |
Conditions
| Conditions | Yield |
|---|---|
| SO4(2-)-TiO2/Al2O3 In N,N-dimethyl-formamide at 80℃; for 6h; | 79% |
Conditions
| Conditions | Yield |
|---|---|
| With pyridine; polymer-supported butyltin(IV) species 1.) MeOH, reflux, 12 h, 2.) DMF, RT, 1 d; Yield given. Multistep reaction. Yields of byproduct given; | |
| With pyridine; polymer-supported butyltin(IV) species 1.) MewOH, reflux, 12 h, 2.) DMF, RT, 1 d; Yield given. Multistep reaction. Yields of byproduct given; |
...Expand
- 63648-81-7
6-O-acetyl sucrose
Conditions
| Conditions | Yield |
|---|---|
| With water; acidic ion exchange resin In N,N-dimethyl-formamide for 0.5h; pH=~ 6; Product distribution / selectivity; | |
| With water; acetic acid In N,N-dimethyl-formamide at 20℃; for 0.5h; pH=6.5; Product distribution / selectivity; |
Conditions
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide at 40 - 50℃; for 6h; Product distribution / selectivity; | |
| In N,N,N,N,N,N-hexamethylphosphoric triamide at 20℃; for 4h; Product distribution / selectivity; | |
| In acetonitrile at 60℃; for 2h; Product distribution / selectivity; |
- 108-24-7
acetic anhydride
- 818-08-6
di(n-butyl)tin oxide
- 57-50-1
Sucrose
A
- 63648-80-6
sucrose 4-acetate
B
- 63648-81-7
6-O-acetyl sucrose
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: di(n-butyl)tin oxide; Sucrose With isopropyl alcohol In N,N-dimethyl-formamide at 100℃; for 5h; Stage #2: acetic anhydride In N,N-dimethyl-formamide at 10 - 27℃; for 6h; Product distribution / selectivity; |
...Expand
Conditions
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide; isopropyl alcohol at 0 - 20℃; for 5.5h; Product distribution / selectivity; |
...Expand
- 108-24-7
acetic anhydride
- 63648-81-7
6-O-acetyl sucrose
Conditions
| Conditions | Yield |
|---|---|
| In N,N-dimethyl-formamide; isopropyl alcohol at 0 - 20℃; Product distribution / selectivity; |
Conditions
| Conditions | Yield |
|---|---|
| Stage #1: 1,3(diO-sucrose)dibutyl stannylene In N,N-dimethyl-formamide at 40 - 45℃; for 0.5h; Stage #2: acetic anhydride In N,N-dimethyl-formamide at 0 - 20℃; for 3 - 4h; Product distribution / selectivity; |
Conditions
| Conditions | Yield |
|---|---|
| diethylazodicarboxylate In N,N-dimethyl-formamide at 20℃; for 5h; Product distribution / selectivity; |
- Total:26 Page 1 of 1 1
Post a RFQ
1
What can I do for you?
Get Best Price
Get Best Price for 63648-81-7
Sucrose-6-acetic ester
