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686-07-7

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Basic Information
CAS No.: 686-07-7
Name: methyl diethyldithiocarbamate
Article Data: 13
Molecular Structure:
Molecular Structure of 686-07-7 (methyl diethyldithiocarbamate)
Formula: C6H13 N S2
Molecular Weight: 163.308
Synonyms: Carbamic acid,diethyldithio-, methyl ester (6CI,7CI,8CI); Carbamodithioic acid, diethyl-,methyl ester (9CI); Diethyldithiocarbamate methyl ester; MethylN,N-diethyldithiocarbamate; Methyl diethyldithiocarbamate; NSC 133269
Density: 1.061g/cm3
Boiling Point: 208.5°C at 760 mmHg
Flash Point: 79.9°C
PSA: 60.63000
LogP: 1.97610
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Synthetic route
75-15-0

carbon disulfide

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diethylamine

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methyl iodide

686-07-7

methyl diethyldithiocarbamate

Conditions
ConditionsYield
at 0 - 20℃;98%
In water at 20℃; for 0.166667h; Sonication;80%
With ethanol
...Expand
148-18-5

sodium N,N-diethyldithiocarbamate

74-88-4

methyl iodide

686-07-7

methyl diethyldithiocarbamate

Conditions
ConditionsYield
In acetone at 0℃; for 12h;82%
In water at 20℃; Kinetics; Further Variations:; Reagents;
148-18-5

sodium N,N-diethyldithiocarbamate

868-85-9

Dimethyl phosphite

686-07-7

methyl diethyldithiocarbamate

Conditions
ConditionsYield
at 100℃; for 4h;
147-84-2

Diethyldithiocarbamic acid

14031-35-7, 17176-17-9, 29908-03-0, 75044-81-4, 78548-84-2, 79647-17-9, 91279-78-6

S-Adenosyl-L-methionine

686-07-7

methyl diethyldithiocarbamate

Conditions
ConditionsYield
With rat hepatic microsomes In phosphate buffer at 37℃; for 0.25h; pH=7.6; Enzyme kinetics; Further Variations:; Reagents; Methylation; Enzymatic reaction;
21124-33-4

ammonium salt of N-diethylamino dithiocarbamic acid

74-88-4

methyl iodide

686-07-7

methyl diethyldithiocarbamate

Conditions
ConditionsYield
In water at 20℃; Kinetics; Further Variations:; Reagents;
2391-78-8

N,N-diethyldithiocarbamate triethylamine salt

74-88-4

methyl iodide

686-07-7

methyl diethyldithiocarbamate

Conditions
ConditionsYield
In acetonitrile at 20℃;
686-07-7

methyl diethyldithiocarbamate

7-tert-butyl-4-hydroxy-6-phenyl-6H-pyrano[3,2-c]pyridine-2,5-dione

3-diethylaminothiocarbonylthio-4-hydroxy-7-t-butyl-6-phenyl-2H-pyrano[3,2-c]pyridine-2,5-dione

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 90℃; Reflux;93%
686-07-7

methyl diethyldithiocarbamate

4-hydroxy-8-methyl-6,7-diphenyl-6H-pyrano[3,2-c]pyridine-2,5-dione

3-diethylaminothiocarbonylthio-8-methyl-4-hydroxy-6,7-diphenyl-2H-pyrano[3,2-c]pyridine-2,5-dione

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 90℃; Reflux;82%
686-07-7

methyl diethyldithiocarbamate

4-hydroxy-7-isopropyl-6-phenyl-6H-pyrano[3,2-c]pyridine-2,5-dione

3-diethylaminothiocarbonylthio-4-hydroxy-7-i-propyl-6-phenyl-2H-pyrano[3,2-c]pyridine-2,5-dione

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 90℃; Reflux;77%
4812-99-1

4-hydroxy-1,6-diphenyl-pyridin-2(1H)-one

686-07-7

methyl diethyldithiocarbamate

3-diethylaminothiocarbonylthio-4-hydroxy-1,6-diphenylpyridin-2(1H)-one

Conditions
ConditionsYield
With potassium carbonate In N,N-dimethyl-formamide at 90℃; for 5h; Reflux;76%
Raw Materials
148-18-5
2391-78-8
868-85-9
21124-33-4
74-88-4
109-89-7
147-84-2
75-15-0
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